Benzenemethanol, 2-methoxy-4-methyl-

Base Information

• Chemical Name: Benzenemethanol, 2-methoxy-4-methyl-
• CAS No.: 10542-80-0
• Molecular Formula: C9H12O2
• Molecular Weight: 152.19000
• Hs Code.: 2909499000
• Mol file: 10542-80-0.mol

Synonyms:

Chemical Property of Benzenemethanol, 2-methoxy-4-methyl-

Chemical Property:

• Boiling Point: 280-290 °C
• PSA: 29.46000
• Density: 1.060±0.06 g/cm3(Predicted)
• LogP: 1.49590

Purity/Quality:

97% ^*data from raw suppliers

2-Methoxy-4-methylbenzylalcohol 96% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, 2-methoxy-4-methyl-

There total 4 articles about Benzenemethanol, 2-methoxy-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

methyl 4-methyl-2-methoxybenzoate (81245-24-1) → (2-methoxy-4-methylphenyl)methanol (10542-80-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1021/ol302371s

Reference yield: 92.0%

2-methoxy-4-methylbenzoic acid (704-45-0) → (2-methoxy-4-methylphenyl)methanol (10542-80-0)

Guidance literature:

With borane-THF; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/acs.jmedchem.7b00785

Reference yield:

2-hydroxy-p-toluic acid (50-85-1) → (2-methoxy-4-methylphenyl)methanol (10542-80-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 18 h / 70 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1021/ol302371s

upstream raw materials:

methyl 4-methyl-2-methoxybenzoate

2-methoxy-4-methylbenzoic acid

2-hydroxy-p-toluic acid

Downstream raw materials:

6-Chloro-9-(2-methoxy-4-methyl-benzyl)-2-trifluoromethyl-9H-purine

1-(2-methoxy-4-methylphenyl)-2-nitropropene

(+/-)-1-(2-methoxy-4-methylphenyl)-2-aminopropane

2-methoxy-3-methyl-β-nitrostyrene

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