Technology Process of (2-methoxy-4-methylphenyl)methanol
There total 4 articles about (2-methoxy-4-methylphenyl)methanol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutylammomium bromide;
In
dichloromethane; water;
at 25 ℃;
for 5h;
Inert atmosphere;
DOI:10.1021/ol302371s
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
2: pyridine; phosphorus tribromide / diethyl ether / 2 h / 50 °C / Inert atmosphere
3: tetrabutylammomium bromide / dichloromethane; water / 5 h / 25 °C / Inert atmosphere
With
pyridine; lithium aluminium tetrahydride; tetrabutylammomium bromide; phosphorus tribromide;
In
tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/ol302371s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetone / 18 h / 70 °C / Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
3: pyridine; phosphorus tribromide / diethyl ether / 2 h / 50 °C / Inert atmosphere
4: tetrabutylammomium bromide / dichloromethane; water / 5 h / 25 °C / Inert atmosphere
With
pyridine; lithium aluminium tetrahydride; tetrabutylammomium bromide; phosphorus tribromide; potassium carbonate;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; acetone;
DOI:10.1021/ol302371s
