1-(1-(4-CHLOROPHENYL)VINYL)BENZENE

Base Information

• Chemical Name: 1-(1-(4-CHLOROPHENYL)VINYL)BENZENE
• CAS No.: 18218-20-7
• Molecular Formula: C14H11 Cl
• Molecular Weight: 214.694
• Mol file: 18218-20-7.mol

Synonyms:Ethylene,1-(p-chlorophenyl)-1-phenyl- (8CI); 1-(p-Chlorophenyl)-1-phenylethene;1-(p-Chlorophenyl)-1-phenylethylene; 1-Chloro-4-(1-phenylethenyl)benzene;1-Phenyl-1-(p-chlorophenyl)ethylene; EGIS 5926

Chemical Property of 1-(1-(4-CHLOROPHENYL)VINYL)BENZENE

Chemical Property:

• Refractive Index: 1.6115 (589.3 nm 28℃)
• Boiling Point: 164 °C(Press: 16 Torr)
• PSA: 0.00000
• Density: 1.107±0.06 g/cm3(Predicted)
• LogP: 4.40150
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1-(1-(4-Chlorophenyl)vinyl)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(1-(4-CHLOROPHENYL)VINYL)BENZENE

There total 54 articles about 1-(1-(4-CHLOROPHENYL)VINYL)BENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + bromochlorobenzene (106-39-8) → (E)-1-(4-chlorophenyl)-2-phenylethene (1657-50-7) + 1-(4-chlorophenyl)-1-phenylethene (18218-20-7)

Guidance literature:

With sodium carbonate; Pd-montmorillonite; In 1-methyl-pyrrolidin-2-one; at 150 ℃; for 2h;

DOI:10.1055/s-2006-951493

Reference yield: 97.0%

4-vinylbenzyl chloride (1073-67-2,24991-47-7) + iodobenzene (591-50-4) → (E)-1-(4-chlorophenyl)-2-phenylethene (1657-50-7) + 1-(4-chlorophenyl)-1-phenylethene (18218-20-7)

Guidance literature:

With [(N-di(2-pyridyl)methyl-N'-cyclohexylurea)PdCl₂]; diisopropylamine; In 1-methyl-pyrrolidin-2-one; water; at 160 ℃; for 32h;

DOI:10.1021/ol0341849

Reference yield: 91.0%

4-vinylbenzyl chloride (1073-67-2,24991-47-7) + iodobenzene (591-50-4) → 1-chloro-4-styrylbenzene (1657-49-4,1657-50-7,4714-23-2,130059-92-6,130059-96-0) + 1-(4-chlorophenyl)-1-phenylethene (18218-20-7)

Guidance literature:

With C₃₂H₂₅ClNO₂PPd; triethylamine; at 130 ℃; for 1.5h; Catalytic behavior; Sealed tube; Green chemistry;

DOI:10.1016/j.mcat.2019.110406

upstream raw materials:

para-chloroacetophenone

methyl magnesium iodide

4-chlorobenzophenone

styrene

Downstream raw materials:

(Z)-1-phenyl-1-(p-chlorophenyl)-2-bromoethylene

(E)-1-(2-bromo-1-phenylvinyl)-4-chlorobenzene

3,8-Bis-phenyl-3,8-bis(p-chlorophenyl)-2,7-dioxaspiro<4,4>nonane-1,6-dione

5-(4-Chloro-phenyl)-benzo[a]anthracene-7,12-dione

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