1,2-Dimethoxy-3-(3-methylbut-2-en-1-yl)benzene

Base Information

• Chemical Name: 1,2-Dimethoxy-3-(3-methylbut-2-en-1-yl)benzene
• CAS No.: 106748-28-1
• Molecular Formula: C13H18O2
• Molecular Weight: 206.285
• DSSTox Substance ID: DTXSID20513723
• Mol file: 106748-28-1.mol

Synonyms:106748-28-1;1,2-Dimethoxy-3-(3-methylbut-2-en-1-yl)benzene;DTXSID20513723

Chemical Property of 1,2-Dimethoxy-3-(3-methylbut-2-en-1-yl)benzene

Chemical Property:

• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 206.130679813
• Heavy Atom Count: 15
• Complexity: 207

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=CCC1=C(C(=CC=C1)OC)OC)C

Technology Process of 1,2-Dimethoxy-3-(3-methylbut-2-en-1-yl)benzene

There total 2 articles about 1,2-Dimethoxy-3-(3-methylbut-2-en-1-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1,2-dimethoxybenzene (91-16-7) + prenyl diisopropyl phosphate (83036-58-2) → 1,2-Dimethoxy-3-(3-methyl-but-2-enyl)-benzene (106748-28-1)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 4h;

DOI:10.1246/cl.1982.797

Reference yield: 5.0%

o-benzoquinone bis(dimethyl acetal) (65492-28-6) + 3-methyl-2-butenyllithium (50585-10-9,86211-76-9) → 2,3-dimethoxy-5-(3-methyl-buten-1-yl)-benzene (83036-42-4) + 4-(1,1-Dimethyl-allyl)-1,2-dimethoxy-benzene (82895-34-9) + 1,2-Dimethoxy-3-(3-methyl-but-2-enyl)-benzene (106748-28-1)

Guidance literature:

In tetrahydrofuran; at -78 ℃; for 0.5h;

DOI:10.1016/S0040-4039(00)87299-8

upstream raw materials:

1,2-dimethoxybenzene

prenyl diisopropyl phosphate

o-benzoquinone bis(dimethyl acetal)

3-methyl-2-butenyllithium

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