N-TRIDECANOPHENONE

Base Information

• Chemical Name: N-TRIDECANOPHENONE
• CAS No.: 6005-99-8
• Molecular Formula: C19H30O
• Molecular Weight: 274.447
• Hs Code.: 2914399090
• Mol file: 6005-99-8.mol

Synonyms:Tridecanophenone(8CI);Dodecyl phenyl ketone;

Chemical Property of N-TRIDECANOPHENONE

Chemical Property:

• Melting Point: 42 °C
• Boiling Point: 374.5 °C at 760 mmHg
• Flash Point: 142 °C
• PSA: 17.07000
• Density: 0.907g/cm³
• LogP: 6.18030

Purity/Quality:

98%,99%, ^*data from raw suppliers

Tridecanophenone >96.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-TRIDECANOPHENONE

There total 41 articles about N-TRIDECANOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(tridec-1-ynyl)benzene → 1-phenyltridecan-1-one (6005-99-8)

Guidance literature:

With iron(III) trifluoromethanesulfonate; trifluorormethanesulfonic acid; In tetrahydrofuran; at 100 ℃; for 12h; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.201701830

Reference yield: 96.0%

C31H52O2 → 1-phenyltridecan-1-one (6005-99-8)

Guidance literature:

With iron(III) trifluoromethanesulfonate; trifluorormethanesulfonic acid; In tetrahydrofuran; at 100 ℃; for 12h; Reagent/catalyst; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.201701830

Reference yield: 95.0%

2-hydroxy-2-phenyltetradecanoic acid (22986-80-7) → 1-phenyltridecan-1-one (6005-99-8)

Guidance literature:

With (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)); oxygen; pivalaldehyde; In acetonitrile; for 2h; Ambient temperature;

DOI:10.1016/S0040-4039(98)00482-1

upstream raw materials:

laurylmagnesium bromide

benzonitrile

n-tridecanoyl chloride

benzene

Downstream raw materials:

1-hydroxytridecylbenzene

2-phenyltetradecan-2-ol

2-Phenyl-1-tetradecene

Benzyl-n-dodecylketon