tetradec-2-en-2-ylbenzene

Base Information

Chemical Name:tetradec-2-en-2-ylbenzene
CAS No.:94681-69-3
Molecular Formula:C₂₀H₃₂
Molecular Weight:272.474
Hs Code.:

Synonyms:tetradec-2-en-2-ylbenzene

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Chemical Property of tetradec-2-en-2-ylbenzene

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Technology Process of tetradec-2-en-2-ylbenzene

There total 7 articles about tetradec-2-en-2-ylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: dodecyltriphenylphosphonium bromide

: 98-86-2
acetophenone

: 94681-69-3
tetradec-2-en-2-ylbenzene

Guidance literature:: dodecyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.75h; Inert atmosphere; Schlenk technique;

acetophenone; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.1c05757

Reference yield:

: 833-81-8,1017-22-7,34473-62-6,85165-70-4,779-51-1
1,2-diphenylpropene

: 94681-69-3
tetradec-2-en-2-ylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mn(dtbpy)₂(OTf)₂; oxygen / methanol; 2,2,2-trifluoroethanol / 12 h / 20 °C / 760.05 Torr / Schlenk technique; Irradiation

2.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere; Schlenk technique

2.2: 20 °C / Inert atmosphere; Schlenk technique

With potassium tert-butylate; oxygen; Mn(dtbpy)₂(OTf)₂; In tetrahydrofuran; methanol; 2,2,2-trifluoroethanol;
DOI:10.1021/jacs.1c05757

Reference yield:

: 98-83-9,6144-04-3,25014-31-7,42612-14-6
isopropenylbenzene

: 94681-69-3
tetradec-2-en-2-ylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mn(dtbpy)₂(OTf)₂; oxygen / methanol; 2,2,2-trifluoroethanol / 12 h / 20 °C / 760.05 Torr / Schlenk technique; Irradiation

2.1: potassium tert-butylate / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere; Schlenk technique

2.2: 20 °C / Inert atmosphere; Schlenk technique

With potassium tert-butylate; oxygen; Mn(dtbpy)₂(OTf)₂; In tetrahydrofuran; methanol; 2,2,2-trifluoroethanol;
DOI:10.1021/jacs.1c05757