2-Methyl-3-phenylbut-3-ene-2-peroxol

Base Information

Chemical Name:2-Methyl-3-phenylbut-3-ene-2-peroxol
CAS No.:108773-57-5
Molecular Formula:C₁₁H₁₄O₂
Molecular Weight:178.231
Hs Code.:
DSSTox Substance ID:DTXSID50597859
Wikidata:Q82493516

Synonyms:108773-57-5;2-Methyl-3-phenylbut-3-ene-2-peroxol;SCHEMBL8578348;DTXSID50597859

Suppliers and Price of 2-Methyl-3-phenylbut-3-ene-2-peroxol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Methyl-3-phenylbut-3-ene-2-peroxol

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:178.099379685
Heavy Atom Count:13
Complexity:179

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C(=C)C1=CC=CC=C1)OO

Technology Process of 2-Methyl-3-phenylbut-3-ene-2-peroxol

There total 5 articles about 2-Methyl-3-phenylbut-3-ene-2-peroxol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-86-2
acetophenone

: 108773-57-5
2-methyl-3-phenylbut-3-ene-2-yl hydroperoxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / diethyl ether / 1 h / Heating

1.2: diethyl ether

2.1: sulfuric acid; acetic acid / 0.07 h / 60 °C

3.1: singlet O₂

With oxygen; sulfuric acid; magnesium; acetic acid; In diethyl ether; 1.1: Grignard reaction;
DOI:10.1021/ol017138m

Reference yield:

: 769-57-3
α,β,β-trimethylstyrene

: 108773-57-5
2-methyl-3-phenylbut-3-ene-2-yl hydroperoxide

: 108773-58-6
2-methyl-3-phenylbut-1-ene-3-yl hydroperoxide

Guidance literature:: With polymer-bound Rose Bengal; oxygen; In tetrachloromethane; for 20h; Title compound not separated from byproducts; Irradiation;
DOI:10.1021/jo00390a033

Reference yield:

: 35947-67-2
3,3,4-trimethyl-4-phenyl-oxetan-2-one

: 108773-57-5
2-methyl-3-phenylbut-3-ene-2-yl hydroperoxide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 140 - 170 °C

2: 74 percent Spectr_. / O₂, polymer-bound Rose Bengal / CCl₄ / 20 h / Irradiation

With polymer-bound Rose Bengal; oxygen; In tetrachloromethane;
DOI:10.1021/jo00390a033