2,3-Dimethyl-6-nitrobenzaldehyde

Base Information

Chemical Name:2,3-Dimethyl-6-nitrobenzaldehyde
CAS No.:109133-82-6
Molecular Formula:C9H9NO3
Molecular Weight:179.175
Hs Code.:
DSSTox Substance ID:DTXSID50552887
Wikidata:Q82433288
Mol file:109133-82-6.mol

Synonyms:2,3-dimethyl-6-nitrobenzaldehyde;109133-82-6;Benzaldehyde, 2,3-dimethyl-6-nitro-;2,3-dimethyl-6nitrobenzaldehyde;SCHEMBL10755226;DTXSID50552887;AGIWNONRDJEVHH-UHFFFAOYSA-N

Suppliers and Price of 2,3-Dimethyl-6-nitrobenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
2,3-Dimethyl-6-nitrobenzaldehyde
5g
$ 1590.00

Total 0 raw suppliers

Chemical Property of 2,3-Dimethyl-6-nitrobenzaldehyde

Chemical Property:

Boiling Point:341.4±30.0 °C(Predicted)
PSA：62.89000
Density:1.231±0.06 g/cm3(Predicted)
LogP:2.54730
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:179.058243149
Heavy Atom Count:13
Complexity:211

Purity/Quality:: 2,3-Dimethyl-6-nitrobenzaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C=C1)[N+](=O)[O-])C=O)C

Technology Process of 2,3-Dimethyl-6-nitrobenzaldehyde

There total 4 articles about 2,3-Dimethyl-6-nitrobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 97135-92-7
2,3-dimethyl-6-nitrobenzenemethanol

: 109133-82-6
2,3-dimethyl-6-nitrobenzaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 4h;
DOI:10.1021/jm00113a033

Reference yield:

: 52911-60-1
2,3-dimethyl-6-nitrobenzonitrile

: 109133-82-6
2,3-dimethyl-6-nitrobenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BH₃-THF, 2.) 10percent HCl / 1.) overnight, 2.) reflux, 30 min

2: 1.) sodium nitrite, acetic acid, 2.) 1 N aq. NaOH / 1.) water, RT, 10 min, 2.) methanol

3: 93 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h

With hydrogenchloride; sodium hydroxide; borane-THF; acetic acid; pyridinium chlorochromate; sodium nitrite; In dichloromethane;
DOI:10.1021/jm00113a033

Reference yield:

: 59146-96-2
2,3-dimethyl-6-nitroaniline

: 109133-82-6
2,3-dimethyl-6-nitrobenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) concd. aq. HCl, sodium nitrite, 2.) copper(I) cyanide / 1.) 5 deg C, 2.) H₂O, RT, overnight

2: 1.) BH₃-THF, 2.) 10percent HCl / 1.) overnight, 2.) reflux, 30 min

3: 1.) sodium nitrite, acetic acid, 2.) 1 N aq. NaOH / 1.) water, RT, 10 min, 2.) methanol

4: 93 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h

With hydrogenchloride; sodium hydroxide; borane-THF; copper(l) cyanide; acetic acid; pyridinium chlorochromate; sodium nitrite; In dichloromethane;
DOI:10.1021/jm00113a033