1-Cyclohexene-1-carboxamide, N-(2-iodophenyl)-N-methyl-

Base Information

Chemical Name:1-Cyclohexene-1-carboxamide, N-(2-iodophenyl)-N-methyl-
CAS No.:109686-67-1
Molecular Formula:C14H16INO
Molecular Weight:341.192
Hs Code.:
DSSTox Substance ID:DTXSID10455981
Nikkaji Number:J1.329.701K
Wikidata:Q82278165
Mol file:109686-67-1.mol

Synonyms:1-Cyclohexene-1-carboxamide, N-(2-iodophenyl)-N-methyl-;109686-67-1;DTXSID10455981;N-Methyl-N-(2-iodophenyl)cyclohexene-1-carboxamide

Suppliers and Price of 1-Cyclohexene-1-carboxamide, N-(2-iodophenyl)-N-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Cyclohexene-1-carboxamide, N-(2-iodophenyl)-N-methyl-

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:341.02766
Heavy Atom Count:17
Complexity:313

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(C1=CC=CC=C1I)C(=O)C2=CCCCC2

Technology Process of 1-Cyclohexene-1-carboxamide, N-(2-iodophenyl)-N-methyl-

There total 4 articles about 1-Cyclohexene-1-carboxamide, N-(2-iodophenyl)-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 552857-09-7
N-(2-iodophenyl)-1-cyclohexene-1-carboxamide

: 74-88-4
methyl iodide

: 109686-67-1
N-(2-iodophenyl)-N-methyl-1-cyclohexene-1-carboxamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.3987/COM-02-S51

Reference yield:

: 636-82-8
cyclohexene-1-carboxylic acid

: 109686-67-1
N-(2-iodophenyl)-N-methyl-1-cyclohexene-1-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / dimethylformamide; CH₂Cl₂ / 4 h / Heating

2: Et₃N / CH₂Cl₂ / 2 h / 50 °C

3: 91 percent / NaH / dimethylformamide / 0.5 h / 20 °C

With oxalyl dichloride; sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/COM-02-S51

Reference yield:

: 36278-22-5
1-cyclohexenoyl chloride

: 109686-67-1
N-(2-iodophenyl)-N-methyl-1-cyclohexene-1-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 2 h / 50 °C

2: 91 percent / NaH / dimethylformamide / 0.5 h / 20 °C

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3987/COM-02-S51