5-Benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione

Base Information

Chemical Name:5-Benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione
CAS No.:109687-35-6
Molecular Formula:C19H18O4
Molecular Weight:310.35
Hs Code.:
DSSTox Substance ID:DTXSID10551053
Wikidata:Q82430566
Mol file:109687-35-6.mol

Synonyms:109687-35-6;5-Benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione;SCHEMBL16174907;DTXSID10551053

Suppliers and Price of 5-Benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:310.12050905
Heavy Atom Count:23
Complexity:436

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(OC(=O)C(C(=O)O1)(CC2=CC=CC=C2)C3=CC=CC=C3)C

Technology Process of 5-Benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione

There total 2 articles about 5-Benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 15231-78-4
2.2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione

: 100-39-0
benzyl bromide

: 109687-35-6
5-benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione

Guidance literature:: With triethylamine; In dimethyl sulfoxide; at 20 ℃;

Reference yield: 88.0%

: 3709-27-1
5-benzyl-2,2-dimethyl-1,3-dioxane-4,6-dione

: 1483-72-3
diphenyliodonium chloride

: 109687-35-6
5-benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; at 70 ℃; for 18h;
DOI:10.1021/jo00227a031

Reference yield: 86.0%

: 488151-80-0
3-(p-methoxyphenyl)-2-propen-1-yl methyl carbonate

: 20671-52-7
lithium pyrrolide

: 109687-35-6
5-benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione

: C₂₉H₂₇NO₂

Guidance literature:: lithium pyrrolide; 5-benzyl-2,2-dimethyl-5-phenyl-1,3-dioxane-4,6-dione; In 1,4-dioxane; for 0.00166667h; Schlenk technique; Inert atmosphere;

3-(p-methoxyphenyl)-2-propen-1-yl methyl carbonate; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 20 ℃; chemoselective reaction; Schlenk technique; Sealed tube; Inert atmosphere;
DOI:10.1039/c4cc07253g