4l5-Trioxaphosphetane,4,4,4-triphenoxy-

Base Information

• Chemical Name: 4l5-Trioxaphosphetane,4,4,4-triphenoxy-
• CAS No.: 29833-83-8
• Molecular Formula: C18H15 O6 P
• Molecular Weight: 358.287

Synonyms:Trioxaphosphetane,4,4-dihydro-4,4,4-triphenoxy- (8CI); Trioxaphosphetane, dihydrotriphenoxy-(9CI); Phosphorous acid, triphenyl ester, ozonide; Triphenyl phosphite ozonide

Chemical Property of 4l5-Trioxaphosphetane,4,4,4-triphenoxy-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4l5-Trioxaphosphetane,4,4,4-triphenoxy-

There total 1 articles about 4l5-Trioxaphosphetane,4,4,4-triphenoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenyl phosphite (101-02-0) → triphenyl phosphite ozonide (29833-83-8)

Guidance literature:

With ozone; In dichloromethane; at -70 ℃; stabilization of ozonides;

DOI:10.1016/S0040-4039(00)86848-3

Reference yield: 42.0%

triphenyl phosphite ozonide (29833-83-8) + 6-isopropylidene-2,2-dimethyl-4-trimethylsiloxy-1,3-dioxine → phosphoric acid triphenyl ester (115-86-6) + 6-(1-hydroxy-1-methyl-ethyl)-2,2-dimethyl-[1,3]dioxin-4-one + 6-(1-hydroperoxy-1-methyl)ethyl-2,2-dimethyl-1,3-dioxin-4-one (345304-95-2) + 6-(1-(diphenylphosphoryl)peroxy-1-methyl)ethyl-2,2-dimethyl-1,3-dioxin-4-one (345305-02-4)

Guidance literature:

With triphenyl phosphite ozonide; In dichloromethane; at -78 - 20 ℃; for 1h; Product distribution;

DOI:10.1021/jo015562v

Reference yield: 21.0%

triphenyl phosphite ozonide (29833-83-8) + 1,1,2-tricyclopropylethene (23603-63-6) → dicyclopropyl ketone (1121-37-5) + Cyclopropanecarboxaldehyde (1489-69-6)

Guidance literature:

In dichloromethane; 1) -78 deg C, 2) -60 deg C, 24h;

DOI:10.1021/jo01303a017

upstream raw materials:

triphenyl phosphite

Downstream raw materials:

trimethyl phosphite

dimethyl phenyl phosphate

phosphoric acid methyl ester diphenyl ester

phosphoric acid triphenyl ester

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