2-(DiMethoxyMethyl)-5-(MethoxyMethyl)furan

Base Information

• Chemical Name: 2-(DiMethoxyMethyl)-5-(MethoxyMethyl)furan
• CAS No.: 110339-34-9
• Molecular Formula: C9H14O4
• Molecular Weight: 186.208
• Mol file: 110339-34-9.mol

Synonyms:Furan,2-(dimethoxymethyl)-5-(methoxymethyl);methoxymethyl-5 dimethoxymethyl-2 furanne;

Chemical Property of 2-(DiMethoxyMethyl)-5-(MethoxyMethyl)furan

Chemical Property:

• Boiling Point: 173.3±35.0 °C(Predicted)
• PSA: 40.83000
• Density: 1.068±0.06 g/cm3(Predicted)
• LogP: 1.71740

Purity/Quality:

99% ^*data from raw suppliers

2-(Dimethoxymethyl)-5-(methoxymethyl)furan ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-(Dimethoxymethyl)-5-(methoxymethyl)furan is used in the study of reaction pathways of glucose during esterifications.

Technology Process of 2-(DiMethoxyMethyl)-5-(MethoxyMethyl)furan

There total 9 articles about 2-(DiMethoxyMethyl)-5-(MethoxyMethyl)furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.4%

methanol (67-56-1) + α-D-fructofuranose (10489-79-9) → 5-hydroxymethyl-2-furfuraldehyde (67-47-0) + 5-(methoxymethyl)-2-furaldehyde (1917-64-2) + levulinic acid methyl ester (624-45-3) + 2-(dimethoxymethyl)-5-(methoxymethyl)furan (110339-34-9)

Guidance literature:

With C₇H₇NO₂*3H⁽¹⁺⁾*O₄₀PW₁₂^(3-); at 120 ℃; for 10h; Reagent/catalyst; Catalytic behavior; Sealed tube;

DOI:10.1039/c8ra02278j

Reference yield: 50.0%

methanol (67-56-1) + D-fructose (470-23-5,470-24-6,10247-46-8,10489-79-9,35673-97-3,36441-90-4,36441-92-6,36468-68-5,37500-17-7,40461-86-7,40461-87-8,41579-20-8,41846-98-4,41846-99-5,41847-00-1,41847-01-2,41847-02-3,41847-03-4,41847-04-5,41847-05-6,41847-06-7,41847-51-2,41847-52-3,42744-42-3) → 5-hydroxymethyl-2-furfuraldehyde (67-47-0) + 5-(methoxymethyl)-2-furaldehyde (1917-64-2) + 5-(hydroxymethyl)-2-(dimethoxymethyl)furan (90200-14-9) + 2-(dimethoxymethyl)-5-(methoxymethyl)furan (110339-34-9)

Guidance literature:

With hydrogenchloride; In water; for 4h; Sealed tube;

Reference yield: 18.0%

methanol (67-56-1) + 5-hydroxymethyl-2-furfuraldehyde (67-47-0) → 2-(dimethoxymethyl)-5-(methoxymethyl)furan (110339-34-9)

Guidance literature:

Amberlite IR 120 (H+); for 15h; Heating;

upstream raw materials:

methanol

5-hydroxymethyl-2-furfuraldehyde

alpha-D-glucopyranose

D-fructose