Phosphonium, [(4-chloro-3-methoxyphenyl)methyl]triphenyl-, bromide

Base Information

Chemical Name:Phosphonium, [(4-chloro-3-methoxyphenyl)methyl]triphenyl-, bromide
CAS No.:110463-12-2
Molecular Formula:C26H23ClOP.Br
Molecular Weight:497.799
Hs Code.:
DSSTox Substance ID:DTXSID80453257
Mol file:110463-12-2.mol

Synonyms:110463-12-2;Phosphonium, [(4-chloro-3-methoxyphenyl)methyl]triphenyl-, bromide;SCHEMBL7084184;DTXSID80453257

Suppliers and Price of Phosphonium, [(4-chloro-3-methoxyphenyl)methyl]triphenyl-, bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphonium, [(4-chloro-3-methoxyphenyl)methyl]triphenyl-, bromide

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:496.03584
Heavy Atom Count:30
Complexity:434

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=CC(=C1)C[P+](C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4)Cl.[Br-]

Technology Process of Phosphonium, [(4-chloro-3-methoxyphenyl)methyl]triphenyl-, bromide

There total 5 articles about Phosphonium, [(4-chloro-3-methoxyphenyl)methyl]triphenyl-, bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 603-35-0
triphenylphosphine

: 103347-14-4
4-(bromomethyl)-1-chloro-2-methoxybenzene

: 110463-12-2
4-chloro-3-methoxyphenylmethyl(triphenyl)phosphonium bromide

Guidance literature:: In benzene; Heating;
DOI:10.1016/S0040-4039(00)85221-1

Reference yield:

: 615-74-7
2-chloro-5-methylphenol

: 110463-12-2
4-chloro-3-methoxyphenylmethyl(triphenyl)phosphonium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / Ambient temperature

2: 62 percent / NBS, AIBN / CCl₄ / Heating

3: 73 percent / toluene / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; In tetrachloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4039(01)80582-7

Reference yield:

: 73909-16-7
2-chloro-5-methylanisole

: 110463-12-2
4-chloro-3-methoxyphenylmethyl(triphenyl)phosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / NBS, AIBN / CCl₄ / Heating

2: 73 percent / toluene / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; toluene;
DOI:10.1016/S0040-4039(01)80582-7