3,5-Pyridinedicarboxylic acid, 2-[[(2-aminoethyl)thio]methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-meth yl-, diethyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 2-[[(2-aminoethyl)thio]methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-meth yl-, diethyl ester
CAS No.:110646-28-1
Molecular Formula:C21H26Cl2N2O4S
Molecular Weight:473.42
Hs Code.:
Mol file:110646-28-1.mol

Synonyms:

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 2-[[(2-aminoethyl)thio]methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-meth yl-, diethyl ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 2-[[(2-aminoethyl)thio]methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-meth yl-, diethyl ester

There total 4 articles about 3,5-Pyridinedicarboxylic acid, 2-[[(2-aminoethyl)thio]methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-meth yl-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156-57-0
2-mercaptoethylamine hydrochloride

: 155497-48-6
2-chloromethyl-3,5-dicarboethoxy-6-methyl-4-(2,3-dichlorophenyl)-6-methyl-1,4-dihydropyridine

: 110646-28-1
2-(2-aminoethylthio)methyl-3,5-dicarboethoxy-4-(2,3-dichlorophenyl)-6-methyl-1,4-dihydropyridine

Guidance literature:: With sodium hydroxide; In 1,2-dimethoxyethane; ethanol; water; at -15 ℃; for 0.25h;
DOI:10.1016/0223-5234(93)90038-G

Reference yield:

: 638-07-3
ethyl (2-chloroaceto)acetate

: 110646-28-1
2-(2-aminoethylthio)methyl-3,5-dicarboethoxy-4-(2,3-dichlorophenyl)-6-methyl-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) benzylamine, acetic acid / 1.) 2-propanol, RT, 24 h, 2.) 2-propanol, RT, 24 h

2: 5 M NaOH / H₂O; ethanol; 1,2-dimethoxy-ethane / 0.25 h / -15 °C

With sodium hydroxide; acetic acid; benzylamine; In 1,2-dimethoxyethane; ethanol; water;
DOI:10.1016/0223-5234(93)90038-G

Reference yield:

: 626-34-6,7318-00-5,41867-20-3
ethyl aminocrotonate

: 110646-28-1
2-(2-aminoethylthio)methyl-3,5-dicarboethoxy-4-(2,3-dichlorophenyl)-6-methyl-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) benzylamine, acetic acid / 1.) 2-propanol, RT, 24 h, 2.) 2-propanol, RT, 24 h

2: 5 M NaOH / H₂O; ethanol; 1,2-dimethoxy-ethane / 0.25 h / -15 °C

With sodium hydroxide; acetic acid; benzylamine; In 1,2-dimethoxyethane; ethanol; water;
DOI:10.1016/0223-5234(93)90038-G