2-Iodo-N-(1,10-phenanthrolin-5-YL)acetamide

Base Information

Chemical Name:2-Iodo-N-(1,10-phenanthrolin-5-YL)acetamide
CAS No.:111047-29-1
Molecular Formula:C14H10IN3O
Molecular Weight:363.15300
Hs Code.:
DSSTox Substance ID:DTXSID40596250
Nikkaji Number:J675.136I
Wikidata:Q82491462
Mol file:111047-29-1.mol

Synonyms:5-iodoacetamido-1,10-phenanthroline;5-iodoacetamido-1,10-phenanthroline-copper;IAAOP;IOP cpd;N-(1,10-phenanthrolin-5-yl)iodacetamide

Suppliers and Price of 2-Iodo-N-(1,10-phenanthrolin-5-YL)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Iodo-N-(1,10-phenanthrolin-5-yl)acetamide 97%
1g
$ 1340.00

Total 0 raw suppliers

Chemical Property of 2-Iodo-N-(1,10-phenanthrolin-5-YL)acetamide

Chemical Property:

Melting Point:180 °C (decomp)(Solv: chloroform (67-66-3))
Boiling Point:591.5±40.0 °C(Predicted)
PSA：58.37000
Density:1.852±0.06 g/cm3(Predicted)
LogP:3.80600
XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:362.98686
Heavy Atom Count:19
Complexity:339

Purity/Quality:: 2-Iodo-N-(1,10-phenanthrolin-5-yl)acetamide 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=CC(=C3C=CC=NC3=C2N=C1)NC(=O)CI
Uses 2-Iodo-N-1,10-phenanthrolin-5-ylacetamide is used in the synthesis of a heterogeneous artificial metallolipase with chimeric catalytic activity.

Technology Process of 2-Iodo-N-(1,10-phenanthrolin-5-YL)acetamide

There total 2 articles about 2-Iodo-N-(1,10-phenanthrolin-5-YL)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 54258-41-2
1,10-phenanthroline-5-amine

: 54907-61-8
iodoacetic anhydride

: 111047-29-1
2-iodo-N-1,10-phenanthrolin-5-ylacetamide

Guidance literature:: In chloroform; Heating;
DOI:10.1016/j.tet.2005.08.012

Reference yield:

: 4199-88-6
5-Nitro-1,10-phenanthroline

: 111047-29-1
2-iodo-N-1,10-phenanthrolin-5-ylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / hydrazine hydrate / 5percent Pd/C / ethanol / 5 h / 70 °C

2: 57 percent

With hydrazine hydrate; palladium on activated charcoal; In ethanol;
DOI:10.1039/ft9938903261