Furan,tetrahydro-2-[3-methoxy-5-(methylsulfonyl)-4-propoxyphenyl]-5-(3,4,5-trimethoxyphenyl)-,(2R,5S)-rel-

Base Information

Chemical Name:Furan,tetrahydro-2-[3-methoxy-5-(methylsulfonyl)-4-propoxyphenyl]-5-(3,4,5-trimethoxyphenyl)-,(2R,5S)-rel-
CAS No.:117065-96-0
Molecular Formula:C₂₄H₃₂O₈S
Molecular Weight:480.579
Hs Code.:

Synonyms:Furan,tetrahydro-2-[3-methoxy-5-(methylsulfonyl)-4-propoxyphenyl]-5-(3,4,5-trimethoxyphenyl)-,cis-(?à)-; Furan,tetrahydro-2-[3-methoxy-5-(methylsulfonyl)-4-propoxyphenyl]-5-(3,4,5-trimethoxyphenyl)-,cis-; L 662418

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Chemical Property of Furan,tetrahydro-2-[3-methoxy-5-(methylsulfonyl)-4-propoxyphenyl]-5-(3,4,5-trimethoxyphenyl)-,(2R,5S)-rel-

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Technology Process of Furan,tetrahydro-2-[3-methoxy-5-(methylsulfonyl)-4-propoxyphenyl]-5-(3,4,5-trimethoxyphenyl)-,(2R,5S)-rel-

There total 8 articles about Furan,tetrahydro-2-[3-methoxy-5-(methylsulfonyl)-4-propoxyphenyl]-5-(3,4,5-trimethoxyphenyl)-,(2R,5S)-rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 116681-60-8
1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanediol

: 106331-88-8,113787-28-3,116681-61-9,116781-15-8,116781-16-9,117065-96-0,121702-59-8,121702-60-1,129314-27-8
(2S,5S)-2-(3-Methanesulfonyl-5-methoxy-4-propoxy-phenyl)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan

: 106331-88-8,113787-28-3,116681-61-9,116781-15-8,116781-16-9,117065-96-0,121702-59-8,121702-60-1,129314-27-8
(2S,5R)-2-(3-Methanesulfonyl-5-methoxy-4-propoxy-phenyl)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan

Guidance literature:: With trifluoroacetic acid; In chloroform; for 0.583333h; Ambient temperature;
DOI:10.1016/S0040-4039(00)82307-2

Reference yield: 23.0%

: 116681-60-8
1-(3-methoxy-5-methylsulfonyl-4-propoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-1,4-butanediol

: 106331-88-8,113787-28-3,116681-61-9,116781-15-8,116781-16-9,117065-96-0,121702-59-8,121702-60-1,129314-27-8
(2S,5S)-2-(3-Methanesulfonyl-5-methoxy-4-propoxy-phenyl)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan

: 106331-88-8,113787-28-3,116681-61-9,116781-15-8,116781-16-9,117065-96-0,121702-59-8,121702-60-1,129314-27-8
(2S,5R)-2-(3-Methanesulfonyl-5-methoxy-4-propoxy-phenyl)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan

Guidance literature:: With trifluoroacetic acid; In chloroform; for 0.583333h; Ambient temperature;
DOI:10.1016/S0040-4039(00)82307-2

Reference yield:

: 1136-86-3
methyl (3,4,5-trimethoxyphenyl) ketone

: 106331-88-8,113787-28-3,116681-61-9,116781-15-8,116781-16-9,117065-96-0,121702-59-8,121702-60-1,129314-27-8
(2S,5S)-2-(3-Methanesulfonyl-5-methoxy-4-propoxy-phenyl)-5-(3,4,5-trimethoxy-phenyl)-tetrahydro-furan

Guidance literature:: Multi-step reaction with 3 steps

2: 100 percent / NaBH₄ / ethanol / 1 h / 70 °C / LiAlH₄, THF, RT, 2 h

3: 50 percent / 5percent CF₃COOH / CHCl₃ / 0.58 h / Ambient temperature

With sodium tetrahydroborate; trifluoroacetic acid; In ethanol; chloroform;
DOI:10.1016/S0040-4039(00)82307-2