Propanamide, 3-[(phenylmethyl)amino]-N-[4-(1,4,5,6-tetrahydro-4-methyl-6-oxo-3-pyrid azinyl)phenyl]-, monohydrobromide

Base Information

Chemical Name:Propanamide, 3-[(phenylmethyl)amino]-N-[4-(1,4,5,6-tetrahydro-4-methyl-6-oxo-3-pyrid azinyl)phenyl]-, monohydrobromide
CAS No.:111794-37-7
Molecular Formula:C21H24N4O2.BrH
Molecular Weight:445.359
Hs Code.:
Mol file:111794-37-7.mol

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Chemical Property of Propanamide, 3-[(phenylmethyl)amino]-N-[4-(1,4,5,6-tetrahydro-4-methyl-6-oxo-3-pyrid azinyl)phenyl]-, monohydrobromide

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Technology Process of Propanamide, 3-[(phenylmethyl)amino]-N-[4-(1,4,5,6-tetrahydro-4-methyl-6-oxo-3-pyrid azinyl)phenyl]-, monohydrobromide

There total 2 articles about Propanamide, 3-[(phenylmethyl)amino]-N-[4-(1,4,5,6-tetrahydro-4-methyl-6-oxo-3-pyrid azinyl)phenyl]-, monohydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 111794-34-4
6-<4-(3-bromopropionamido)phenyl>-5-methyl-4,5-dihydro-3(2H)-pyridazinone

: 100-46-9
benzylamine

: 111794-37-7
6-<4-<3-(benzylamino)propionamido>phenyl>-5-methyl-4,5-dihydro-3(2H)-pyridazinone hydrobromide

Guidance literature:: In propan-1-ol; for 6h; Heating;
DOI:10.1021/jm00397a013

Reference yield:

: 36725-28-7
6-(4-aminophenyl)-4,5-dihydro-5-methyl-3(2H)-pyridazinone

: 111794-37-7
6-<4-<3-(benzylamino)propionamido>phenyl>-5-methyl-4,5-dihydro-3(2H)-pyridazinone hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / acetonitrile / 3 h / Heating

2: 81 percent / propan-1-ol / 6 h / Heating

In propan-1-ol; acetonitrile;
DOI:10.1021/jm00397a013