1,3,5,2,4,6-Triazatriphosphorine, 2,2,4,4-tetrachloro-2,2,4,4,6,6-hexahydro-6-hydroxy-6-[(4-methylphenyl) amino]-, compd. with N,N-diethylethanamine (1:1)

Base Information

• Chemical Name: 1,3,5,2,4,6-Triazatriphosphorine, 2,2,4,4-tetrachloro-2,2,4,4,6,6-hexahydro-6-hydroxy-6-[(4-methylphenyl) amino]-, compd. with N,N-diethylethanamine (1:1)
• CAS No.: 112159-82-7
• Molecular Formula: C₆H₁₅N*C₇H₉Cl₄N₄OP₃
• Molecular Weight: 501.1

Synonyms:

Chemical Property of 1,3,5,2,4,6-Triazatriphosphorine, 2,2,4,4-tetrachloro-2,2,4,4,6,6-hexahydro-6-hydroxy-6-[(4-methylphenyl) amino]-, compd. with N,N-diethylethanamine (1:1)

Chemical Property:

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Technology Process of 1,3,5,2,4,6-Triazatriphosphorine, 2,2,4,4-tetrachloro-2,2,4,4,6,6-hexahydro-6-hydroxy-6-[(4-methylphenyl) amino]-, compd. with N,N-diethylethanamine (1:1)

There total 1 articles about 1,3,5,2,4,6-Triazatriphosphorine, 2,2,4,4-tetrachloro-2,2,4,4,6,6-hexahydro-6-hydroxy-6-[(4-methylphenyl) amino]-, compd. with N,N-diethylethanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(2,4,4,6,6-Pentachloro-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinin-2-yl)-p-tolyl-amine (4308-66-1) + triethylamine (121-44-8) → 4,4,6,6-Tetrachloro-2-p-tolylamino-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinin-2-ol; compound with triethyl-amine (112159-82-7)

Guidance literature:

In tetrahydrofuran; for 6h;

Reference yield:

4,4,6,6-Tetrachloro-2-p-tolylamino-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinin-2-ol; compound with triethyl-amine (112159-82-7) → 4,4,6,6-Tetrakis-dimethylamino-2-p-tolylamino-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinin-2-ol; compound with triethyl-amine (112159-86-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CHCl₃

2: 90 percent / CH₂Cl₂

In dichloromethane; chloroform;

Reference yield:

4,4,6,6-Tetrachloro-2-p-tolylamino-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinin-2-ol; compound with triethyl-amine (112159-82-7) + dimethyl amine (124-40-3) → C15H33N8OP3 (112159-84-9)

Guidance literature:

In chloroform;

upstream raw materials:

(2,4,4,6,6-Pentachloro-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinin-2-yl)-p-tolyl-amine

triethylamine

Downstream raw materials:

C₁₅H₃₃N₈OP₃

4,4,6,6-Tetrakis-dimethylamino-2-p-tolylamino-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinin-2-ol; compound with triethyl-amine

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