Silane, trimethyl(3,4,5-trimethylphenyl)-

Base Information

Chemical Name:Silane, trimethyl(3,4,5-trimethylphenyl)-
CAS No.:112277-74-4
Molecular Formula:C12H20Si
Molecular Weight:192.376
Hs Code.:

Synonyms:

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Chemical Property of Silane, trimethyl(3,4,5-trimethylphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Silane, trimethyl(3,4,5-trimethylphenyl)-

There total 7 articles about Silane, trimethyl(3,4,5-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 526-73-8
1,2,3-trimethylbenzene

: 112277-74-4
Trimethyl-(3,4,5-trimethyl-phenyl)-silane

Guidance literature:: Multi-step reaction with 6 steps

1: 50 percent / butyllithium in ether / -60 °C

2: 1.) SOCl₂; 2.) NaN₃ in water, tetrabutylammonium bromide / 1.) methylene dichloride; 2.) 0 deg C, 2 h

3: 1.) trifluoroacetic acid; 2.) K₂CO₃ / 1.) CHCl₂, reflux, 6 h; 2.) aq. methanol, 20 h

4: 75 percent / NBS / dimethylformamide / 24 h

5: 1.) conc. HCl, aq. NaNO₂; 2.) 50percent H₃PO₃ / 1.) acetic anhydride; 2.) 0 deg C, 1 h

6: 1.) BuLi / 1.) ether, 0 deg C; 2.) reflux, 5 h

With hydrogenchloride; N-Bromosuccinimide; n-butyllithium; phosphonic Acid; thionyl chloride; sodium azide; tetrabutylammomium bromide; potassium carbonate; trifluoroacetic acid; sodium nitrite; In N,N-dimethyl-formamide;

Reference yield:

: 1076-47-7
trimethylbenzoic acid

: 112277-74-4
Trimethyl-(3,4,5-trimethyl-phenyl)-silane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) SOCl₂; 2.) NaN₃ in water, tetrabutylammonium bromide / 1.) methylene dichloride; 2.) 0 deg C, 2 h

2: 1.) trifluoroacetic acid; 2.) K₂CO₃ / 1.) CHCl₂, reflux, 6 h; 2.) aq. methanol, 20 h

3: 75 percent / NBS / dimethylformamide / 24 h

4: 1.) conc. HCl, aq. NaNO₂; 2.) 50percent H₃PO₃ / 1.) acetic anhydride; 2.) 0 deg C, 1 h

5: 1.) BuLi / 1.) ether, 0 deg C; 2.) reflux, 5 h

With hydrogenchloride; N-Bromosuccinimide; n-butyllithium; phosphonic Acid; thionyl chloride; sodium azide; tetrabutylammomium bromide; potassium carbonate; trifluoroacetic acid; sodium nitrite; In N,N-dimethyl-formamide;

Reference yield:

: 1467-35-2
2,3,4-trimethylaniline

: 112277-74-4
Trimethyl-(3,4,5-trimethyl-phenyl)-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / NBS / dimethylformamide / 24 h

2: 1.) conc. HCl, aq. NaNO₂; 2.) 50percent H₃PO₃ / 1.) acetic anhydride; 2.) 0 deg C, 1 h

3: 1.) BuLi / 1.) ether, 0 deg C; 2.) reflux, 5 h

With hydrogenchloride; N-Bromosuccinimide; n-butyllithium; phosphonic Acid; sodium nitrite; In N,N-dimethyl-formamide;