Stannane, tributyl(1-phenyl-1-propenyl)-, (E)-

Base Information

Chemical Name:Stannane, tributyl(1-phenyl-1-propenyl)-, (E)-
CAS No.:112713-91-4
Molecular Formula:C₂₁H₃₆Sn
Molecular Weight:407.227
Hs Code.:

Synonyms:

Suppliers and Price of Stannane, tributyl(1-phenyl-1-propenyl)-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Stannane, tributyl(1-phenyl-1-propenyl)-, (E)-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Stannane, tributyl(1-phenyl-1-propenyl)-, (E)-

There total 3 articles about Stannane, tributyl(1-phenyl-1-propenyl)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 673-32-5
1-Phenylprop-1-yne

: 688-73-3
tri-n-butyl-tin hydride

: 124582-43-0,131428-21-2
(E)-tributyl(1-phenylprop-1-en-2-yl)stannane

: 112713-91-4,125405-88-1
E-tributyl-1-phenyl-propenylstannane

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; hydrostannylation, at room temperature, mixture was stood for 10 minutes; removal of solvent (vacuo), flash chromy. (silica gel, dichloromethane);

Reference yield:

: 673-32-5
1-Phenylprop-1-yne

: 688-73-3
tri-n-butyl-tin hydride

: 125405-88-1,112713-91-4
tributyl(1-phenylprop-1-en-1-yl)stannane

: 124582-43-0,131428-21-2
(Z)-tributyl(1-phenylprop-1-en-2-yl)stannane

Guidance literature:: With C₃₃H₄₆PRuS⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-); In chlorobenzene; at 80 ℃; for 24h; Glovebox; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.7b13088

Reference yield:

: 673-32-5
1-Phenylprop-1-yne

: 688-73-3
tri-n-butyl-tin hydride

: 124582-43-0,131428-21-2
(E)-tributyl(1-phenylprop-1-en-2-yl)stannane

: 125405-88-1,112713-91-4
1-(tributylstannyl)-1-phenyl-1-propene

Guidance literature:: With [MoI₂(CO)2(CNC₆H₃(C₆H₃iPr₂-2,6)2-2,6)2]; In benzene-d6; at 20 ℃; for 0.5h; Overall yield = 94 %; Overall yield = 114 mg; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1002/anie.201802397