Benzenemethanesulfenamide, a-phenyl-a-(trifluoromethyl)-

Base Information

Chemical Name:Benzenemethanesulfenamide, a-phenyl-a-(trifluoromethyl)-
CAS No.:112882-16-3
Molecular Formula:C14H12F3NS
Molecular Weight:283.317
Hs Code.:

Synonyms:

Suppliers and Price of Benzenemethanesulfenamide, a-phenyl-a-(trifluoromethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzenemethanesulfenamide, a-phenyl-a-(trifluoromethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenemethanesulfenamide, a-phenyl-a-(trifluoromethyl)-

There total 5 articles about Benzenemethanesulfenamide, a-phenyl-a-(trifluoromethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 112881-92-2
2,2,2-trifluoro-1,1-diphenylethane-sulfenyl chloride

: 112882-16-3
2,2,2-trifluoro-1,1-diphenylethanesulfenamide

Guidance literature:: With ammonium hydroxide; In dichloromethane; for 0.0833333h; Ambient temperature;
DOI:10.1055/s-1987-28045

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 112882-16-3
2,2,2-trifluoro-1,1-diphenylethanesulfenamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Mg / 1.) ether, 2.) reflux, 1 h

2: 1.) NaH / 1.) ether, room temp., 1 h, 2.) room temp., 70 h

3: 96 percent / H₂S, p-TsOH / various solvent(s) / 1 h / 60 °C

4: 96 percent / sulfuryl chloride / diethyl ether / 0.25 h / Ambient temperature

5: 95 percent / 25percent aq. NH₃ / CH₂Cl₂ / 0.08 h / Ambient temperature

With ammonium hydroxide; sulfuryl dichloride; hydrogen sulfide; sodium hydride; toluene-4-sulfonic acid; magnesium; In diethyl ether; dichloromethane;
DOI:10.1055/s-1987-28045

Reference yield:

: 379-18-0
1,1-diphenyl-2,2,2-trifluoroethanol

: 112882-16-3
2,2,2-trifluoro-1,1-diphenylethanesulfenamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) ether, room temp., 1 h, 2.) room temp., 70 h

2: 96 percent / H₂S, p-TsOH / various solvent(s) / 1 h / 60 °C

3: 96 percent / sulfuryl chloride / diethyl ether / 0.25 h / Ambient temperature

4: 95 percent / 25percent aq. NH₃ / CH₂Cl₂ / 0.08 h / Ambient temperature

With ammonium hydroxide; sulfuryl dichloride; hydrogen sulfide; sodium hydride; toluene-4-sulfonic acid; In diethyl ether; dichloromethane;
DOI:10.1055/s-1987-28045