1,1-Dimethoxy-2,2-dimethyldecane

Base Information

• Chemical Name: 1,1-Dimethoxy-2,2-dimethyldecane
• CAS No.: 113138-63-9
• Molecular Formula: C14H30O2
• Molecular Weight: 230.391
• DSSTox Substance ID: DTXSID40550418
• Wikidata: Q82429778
• Mol file: 113138-63-9.mol

Synonyms:1,1-DIMETHOXY-2,2-DIMETHYLDECANE;113138-63-9;DTXSID40550418;2-octyl-2-methyl-dimethoxypropane

Chemical Property of 1,1-Dimethoxy-2,2-dimethyldecane

Chemical Property:

• XLogP3: 5.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 10
• Exact Mass: 230.224580195
• Heavy Atom Count: 16
• Complexity: 151

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCC(C)(C)C(OC)OC

Technology Process of 1,1-Dimethoxy-2,2-dimethyldecane

There total 1 articles about 1,1-Dimethoxy-2,2-dimethyldecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 2,2-dimethyldecanal (14250-93-2) → 2,2-dimethyldecanal dimethyl acetal (113138-63-9)

Guidance literature:

With camphor-10-sulfonic acid; In dichloromethane; at 20 ℃;

DOI:10.1039/c1cc13919c

Reference yield: 100.0%

tributyltin phenyl sulfide (17314-33-9) + 2,2-dimethyldecanal dimethyl acetal (113138-63-9) → 2,2-dimethyl-1-methoxy-1-phenylthiodecane (113138-65-1)

Guidance literature:

With boron trifluoride diethyl etherate; In toluene; addn. of BF3*OEt2 in toluene to the acetal in toluene at -20°C and stirring for 1 h; GLC analysis;

DOI:10.1246/cl.1987.1661

Reference yield:

trimethylsilyl trifluoromethanesulfonate (27607-77-8) + 2,2-dimethyldecanal dimethyl acetal (113138-63-9) + triphenylphosphine (603-35-0) → CF3O3S(1-)*C31H42OP(1+)

Guidance literature:

With air; In dichloromethane; at 0 ℃; for 0.5h; Schlenk technique;

DOI:10.1002/chem.201200480

upstream raw materials:

methanol

2,2-dimethyldecanal

Downstream raw materials:

2,2-dimethyl-1-methoxy-1-phenylthiodecane