1-Methyl-3-methylidenecyclohexane-1-carbonitrile

Base Information

Chemical Name:1-Methyl-3-methylidenecyclohexane-1-carbonitrile
CAS No.:113426-72-5
Molecular Formula:C9H13N
Molecular Weight:135.209
Hs Code.:
DSSTox Substance ID:DTXSID70551993

Synonyms:1-Methyl-3-methylidenecyclohexane-1-carbonitrile;113426-72-5;DTXSID70551993

Suppliers and Price of 1-Methyl-3-methylidenecyclohexane-1-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-Methyl-3-methylidenecyclohexane-1-carbonitrile

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:135.104799419
Heavy Atom Count:10
Complexity:196

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(CCCC(=C)C1)C#N

Technology Process of 1-Methyl-3-methylidenecyclohexane-1-carbonitrile

There total 1 articles about 1-Methyl-3-methylidenecyclohexane-1-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 33235-14-2
1-methyl-3-oxocyclohexane-1-carbonitrile

: 1779-49-3
Methyltriphenylphosphonium bromide

: 113426-72-5
1-cyano-1-methyl-3-methylenecyclohexane

Guidance literature:: With n-butyllithium; 1.) Et₂O-hexane, 10 min, 2.) 5 h;

Reference yield: 46.0%

: 113426-72-5
1-cyano-1-methyl-3-methylenecyclohexane

: 36370-86-2
1-methyl-3-methylenecyclohexanecarboxylic acid

Guidance literature:: With potassium hydroxide; In diethylene glycol; at 200 ℃; for 15h;

Reference yield:

: 113426-72-5
1-cyano-1-methyl-3-methylenecyclohexane

: 1-Methyl-3-methylene-cyclohexanecarbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 46 percent / KOH / bis-(2-hydroxy-ethyl) ether / 15 h / 200 °C

2: 1.) NaOMe, 2.) oxalyl chloride, pyridine / 1.) MeOH, 2.) benzene, 0 deg C, 0.5 h

With pyridine; potassium hydroxide; oxalyl dichloride; sodium methylate; In diethylene glycol;