1-methyl-3-oxocyclohexanecarbonitrile

Base Information

Chemical Name:1-methyl-3-oxocyclohexanecarbonitrile
CAS No.:33235-14-2
Molecular Formula:C8H11NO
Molecular Weight:137.181
Hs Code.:2914290090
Mol file:33235-14-2.mol

Synonyms:3-cyano-3-methylcyclohexanone;(+/-)-3-Oxo-1-methyl-cyclohexan-carbonsaeure-(1)-nitril;1-methyl-3-oxo-cyclohexanecarbonitrile;1-Methyl-3-oxo-cyclohexancarbonitril;

Suppliers and Price of 1-methyl-3-oxocyclohexanecarbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-methyl-3-oxocyclohexanecarbonitrile

Chemical Property:

Boiling Point:152 °C(Press: 19 Torr)
PSA：40.86000
Density:1.02±0.1 g/cm3(Predicted)
LogP:1.65938

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-methyl-3-oxocyclohexanecarbonitrile

There total 11 articles about 1-methyl-3-oxocyclohexanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1193-18-6
3-methylcyclohexen-2-one

: 7677-24-9
trimethylsilyl cyanide

: 33235-14-2
1-methyl-3-oxocyclohexane-1-carbonitrile

Guidance literature:: 3-methylcyclohexen-2-one; trimethylsilyl cyanide; With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; bicyclo[2.2.1]hepta-2,5-diene; gadolinium(III) trifluoromethanesulfonate; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;

Acidic conditions;
DOI:10.1055/s-2008-1078264