2,4-Dimethyl-7-(1-oxopropyl)-2H-1,4-benzoxazin-3(4H)-one

Base Information

Chemical Name:2,4-Dimethyl-7-(1-oxopropyl)-2H-1,4-benzoxazin-3(4H)-one
CAS No.:134577-30-3
Molecular Formula:C13H15NO3
Molecular Weight:233.2631
Hs Code.:
DSSTox Substance ID:DTXSID00928679
Nikkaji Number:J372.139F
Mol file:134577-30-3.mol

Synonyms:BRN 4354928;2,4-Dimethyl-7-(1-oxopropyl)-2H-1,4-benzoxazin-3(4H)-one;2H-1,4-Benzoxazin-3(4H)-one, 2,4-dimethyl-7-(1-oxopropyl)-;134577-30-3;DTXSID00928679;LS-41983;2,4-Dimethyl-7-propanoyl-2H-1,4-benzoxazin-3(4H)-one;2,4-Dimethyl-7-propionyl-4H-1,4-benzoxazin-3(2H)-one

Suppliers and Price of 2,4-Dimethyl-7-(1-oxopropyl)-2H-1,4-benzoxazin-3(4H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2,4-Dimethyl-7-(1-oxopropyl)-2H-1,4-benzoxazin-3(4H)-one

Chemical Property:

Vapor Pressure:2.87E-09mmHg at 25°C
Boiling Point:477.2°Cat760mmHg
Flash Point:242.4°C
Density:1.149g/cm³
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:233.10519334
Heavy Atom Count:17
Complexity:329

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=O)C1=CC2=C(C=C1)N(C(=O)C(O2)C)C

Technology Process of 2,4-Dimethyl-7-(1-oxopropyl)-2H-1,4-benzoxazin-3(4H)-one

There total 3 articles about 2,4-Dimethyl-7-(1-oxopropyl)-2H-1,4-benzoxazin-3(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 7623-09-8
2-chloropropionyl chloride

: 54903-58-1
1-(3-Hydroxy-4-methylamino-phenyl)-propan-1-one

: 134577-30-3
2,4-Dimethyl-7-propionyl-4H-benzo[1,4]oxazin-3-one

Guidance literature:: With sodium hydrogencarbonate; In water; butanone; at 90 ℃; for 8h;

Reference yield:

: 21892-80-8
3-methylbenzo[d]oxazol-2(3H)-one

: 134577-30-3
2,4-Dimethyl-7-propionyl-4H-benzo[1,4]oxazin-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / polyphosphoric acid / 1 h / 90 - 95 °C

2: 90 percent / aq. sodium hydroxide / Heating

3: 76 percent / sodium hydrogencarbonate / butan-2-one; H₂O / 8 h / 90 °C

With sodium hydroxide; PPA; sodium hydrogencarbonate; In water; butanone;

Reference yield:

: 54943-19-0
3-methyl-6-propionyl-3H-benzooxazol-2-one

: 134577-30-3
2,4-Dimethyl-7-propionyl-4H-benzo[1,4]oxazin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / aq. sodium hydroxide / Heating

2: 76 percent / sodium hydrogencarbonate / butan-2-one; H₂O / 8 h / 90 °C

With sodium hydroxide; sodium hydrogencarbonate; In water; butanone;