1,3-Benzenedicarboxylic acid, 5,5'-[[2-(ethoxycarbonyl)-1,3-phenylene]bis(methyleneoxy)]bis-, tetrakis(diphenylmethyl) ester

Base Information

Chemical Name:1,3-Benzenedicarboxylic acid, 5,5'-[[2-(ethoxycarbonyl)-1,3-phenylene]bis(methyleneoxy)]bis-, tetrakis(diphenylmethyl) ester
CAS No.:113597-93-6
Molecular Formula:C79H62O12
Molecular Weight:1203.35
Hs Code.:
Mol file:113597-93-6.mol

Synonyms:

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Chemical Property of 1,3-Benzenedicarboxylic acid, 5,5'-[[2-(ethoxycarbonyl)-1,3-phenylene]bis(methyleneoxy)]bis-, tetrakis(diphenylmethyl) ester

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Technology Process of 1,3-Benzenedicarboxylic acid, 5,5'-[[2-(ethoxycarbonyl)-1,3-phenylene]bis(methyleneoxy)]bis-, tetrakis(diphenylmethyl) ester

There total 6 articles about 1,3-Benzenedicarboxylic acid, 5,5'-[[2-(ethoxycarbonyl)-1,3-phenylene]bis(methyleneoxy)]bis-, tetrakis(diphenylmethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 113585-50-5
ethyl 2,6-bis(bromomethyl)benzoate

: 113585-51-6
bis(diphenylmethyl) 5-hydroxyisophthalate

: 113597-93-6
ethyl 2,6-bis((3,5-bis((diphenylmethoxy)carbonyl)phenoxy)methyl)benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 4h;
DOI:10.1021/ja00219a023

Reference yield:

: 632-46-2
2,6-dimethylbenzoic acid

: 113597-93-6
ethyl 2,6-bis((3,5-bis((diphenylmethoxy)carbonyl)phenoxy)methyl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / dimethylformamide / 4 h / Ambient temperature

2: 8.7 g / Et₃N / CH₂Cl₂ / 1 h

3: 23 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 3 h / Heating

4: 95 percent / K₂CO₃ / dimethylformamide / 4 h

With N-Bromosuccinimide; thionyl chloride; Perbenzoic acid; potassium carbonate; triethylamine; In tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00219a023

Reference yield:

: 36596-67-5
2,6-dimethylbenzoic acid ethyl ester

: 113597-93-6
ethyl 2,6-bis((3,5-bis((diphenylmethoxy)carbonyl)phenoxy)methyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 23 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 3 h / Heating

2: 95 percent / K₂CO₃ / dimethylformamide / 4 h

With N-Bromosuccinimide; Perbenzoic acid; potassium carbonate; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00219a023