[1,1'-Biphenyl]-2-sulfonamide,4'-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]-

Base Information

Chemical Name:[1,1'-Biphenyl]-2-sulfonamide,4'-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]-
CAS No.:145004-89-3
Molecular Formula:C23H24 N4 O2 S
Molecular Weight:420.535
Hs Code.:

Synonyms:3H-Imidazo[4,5-b]pyridine,[1,1'-biphenyl]-2-sulfonamide deriv.; L 159221

Suppliers and Price of [1,1'-Biphenyl]-2-sulfonamide,4'-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,1'-Biphenyl]-2-sulfonamide,4'-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of [1,1'-Biphenyl]-2-sulfonamide,4'-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]-

There total 10 articles about [1,1'-Biphenyl]-2-sulfonamide,4'-[(2-ethyl-5,7-dimethyl-3H-imidazo[4,5-b]pyridin-3-yl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 145004-88-2
4'-(2-Ethyl-5,7-dimethyl-imidazo[4,5-b]pyridin-3-ylmethyl)-biphenyl-2-sulfonic acid tert-butylamide

: 145004-89-3
3-<<2'-aminosulfonyl><1,1'-biphenyl-4-yl>-methyl>-5,7-dimethyl-2-ethyl-imidazo<4,5-b>pyridine

Guidance literature:: With trifluoroacetic acid; at 25 ℃; for 8h;
DOI:10.1021/jm00050a002

Reference yield: 72.0%

: 4'-(2-Ethyl-5,7-dimethyl-imidazo[4,5-b]pyridin-3-ylmethyl)-biphenyl-2-sulfonic acid 1-dimethylamino-meth-(E)-ylideneamide

: 145004-89-3
3-<<2'-aminosulfonyl><1,1'-biphenyl-4-yl>-methyl>-5,7-dimethyl-2-ethyl-imidazo<4,5-b>pyridine

Guidance literature:: With hydrogenchloride; In ethanol; for 2h; Heating;
DOI:10.1016/S0968-0896(97)00012-6

Reference yield:

: 133240-06-9
5,7-dimethyl-2-ethyl-3H-imidazo[4,5-b]pyridine

: 145004-89-3
3-<<2'-aminosulfonyl><1,1'-biphenyl-4-yl>-methyl>-5,7-dimethyl-2-ethyl-imidazo<4,5-b>pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Cs₂CO₃ / dimethylformamide / 24 h / Ambient temperature

2: 72 percent / conc. aq. HCl / ethanol / 2 h / Heating

With hydrogenchloride; caesium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(97)00012-6