Methyl 4-acetyl-3-bromobenzoate

Base Information

Chemical Name:Methyl 4-acetyl-3-bromobenzoate
CAS No.:113642-06-1
Molecular Formula:C10H9BrO3
Molecular Weight:257.084
Hs Code.:
DSSTox Substance ID:DTXSID301304286
Mol file:113642-06-1.mol

Synonyms:methyl 4-acetyl-3-bromobenzoate;113642-06-1;SCHEMBL17888585;DDRZJZKSFMZWHX-UHFFFAOYSA-N;DTXSID301304286

Suppliers and Price of Methyl 4-acetyl-3-bromobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Methyl 4-acetyl-3-bromobenzoate

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:255.97351
Heavy Atom Count:14
Complexity:240

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C1=C(C=C(C=C1)C(=O)OC)Br

Technology Process of Methyl 4-acetyl-3-bromobenzoate

There total 3 articles about Methyl 4-acetyl-3-bromobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 113642-07-2
2-bromo-4-carboxyacetophenone

: 74-88-4
methyl iodide

: 113642-06-1
methyl p-acetyl-m-bromobenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield: 49.0%

: 113642-05-0
methyl m-bromo-p-ethylbenzoate

: 113642-06-1
methyl p-acetyl-m-bromobenzoate

Guidance literature:: With chromium(VI) oxide; In water; acetic acid; for 20h; Ambient temperature;

Reference yield:

: 99548-53-5
3-Bromo-4-ethylbenzoic acid

: 113642-06-1
methyl p-acetyl-m-bromobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / borontrifluoride / diethyl ether / 3 h / Heating

2: 49 percent / CrO₃ / acetic acid; H₂O / 20 h / Ambient temperature

With chromium(VI) oxide; boron trifluoride; In diethyl ether; water; acetic acid;