S-tert-butyl chloroethanethioate

Base Information

Chemical Name:S-tert-butyl chloroethanethioate
CAS No.:56377-45-8
Molecular Formula:C₆H₁₁ClOS
Molecular Weight:166.672
Hs Code.:

Synonyms:

Suppliers and Price of S-tert-butyl chloroethanethioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-tert-butyl chloroethanethioate

Chemical Property:

Vapor Pressure:0.544mmHg at 25°C
Boiling Point:190.3°Cat760mmHg
Flash Point:68.9°C
Density:1.11g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of S-tert-butyl chloroethanethioate

There total 1 articles about S-tert-butyl chloroethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-66-1
2-methylpropan-2-thiol

: 79-04-9
chloroacetyl chloride

: 56377-45-8
Chlorthioessigsaeure-S-tert-butylester

Guidance literature:: at 60 - 90 ℃;
DOI:10.1021/ja01197a502

Reference yield:

: S-chloroacetyl-t-butyl mercaptan

: 56377-45-8
Chlorthioessigsaeure-S-tert-butylester

: 256346-26-6
4-(nicotinoylamidomethyl)-benzenesulfonamide

: 4-[1-(t-butylthiocarbonylmethyl)nicotinamidomethyl]-benzenesulfonamide chloride

Guidance literature:: S-chloroacetyl-t-butyl mercaptan; Chlorthioessigsaeure-S-tert-butylester; 4-(nicotinoylamidomethyl)-benzenesulfonamide; Heating / reflux;

Heating / reflux;

Reference yield:

: 56377-45-8
Chlorthioessigsaeure-S-tert-butylester

: 112303-67-0
S-tert-butyl (3R)-3-hydroxy-3-phenylpropanethioate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) boron - (-)-menthone reagent, Et₃N / 1.) Et₂O, CH₂Cl₂, 5 min at 0 deg C, 5.0 h at 15 deg C, 2.) Et₂O, CH₂Cl₂, -78 deg C, 15 h

2: Zn, NH₄Cl / methanol

With boron - (-)-menthone reagent; ammonium chloride; triethylamine; zinc; In methanol;
DOI:10.1016/S0040-4039(00)76987-5