Phosphonic acid, [2-methoxy-2-[(4-methylphenyl)sulfonyl]ethenyl]-, diethyl ester, (Z)-

Base Information

Chemical Name:Phosphonic acid, [2-methoxy-2-[(4-methylphenyl)sulfonyl]ethenyl]-, diethyl ester, (Z)-
CAS No.:114070-94-9
Molecular Formula:C₁₄H₂₁O₆PS
Molecular Weight:348.357
Hs Code.:
Mol file:114070-94-9.mol

Synonyms:

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Chemical Property of Phosphonic acid, [2-methoxy-2-[(4-methylphenyl)sulfonyl]ethenyl]-, diethyl ester, (Z)-

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Technology Process of Phosphonic acid, [2-methoxy-2-[(4-methylphenyl)sulfonyl]ethenyl]-, diethyl ester, (Z)-

There total 8 articles about Phosphonic acid, [2-methoxy-2-[(4-methylphenyl)sulfonyl]ethenyl]-, diethyl ester, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4851-51-8
diethyl ethynylphosphonate

: 114070-94-9,114070-95-0
diethyl 2-methoxy-2-p-tolylsulphonylvinylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: t-butyl hypochlorite

2: potassium hydroxyde / ethanol / 0.05 h / 0 °C

3: 3-chloroperbenzoic acid / CHCl₃ / 0 deg C, overnight

4: sodium hydride / 0.75 h / Ambient temperature

With potassium hydroxide; tert-butylhypochlorite; 3-chloro-benzenecarboperoxoic acid; sodium hydride; In ethanol; chloroform;

Reference yield:

: 4851-52-9
chloroethynyl-phosphonic acid diethyl ester

: 114070-94-9,114070-95-0
diethyl 2-methoxy-2-p-tolylsulphonylvinylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxyde / ethanol / 0.05 h / 0 °C

2: 3-chloroperbenzoic acid / CHCl₃ / 0 deg C, overnight

3: sodium hydride / 0.75 h / Ambient temperature

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; sodium hydride; In ethanol; chloroform;

Reference yield:

: 66823-38-9
1-ethynylsulfanyl-4-methyl-benzene

: 114070-94-9,114070-95-0
diethyl 2-methoxy-2-p-tolylsulphonylvinylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) butyl-lithium / 1.) tetrahydrofuran, -78 deg C, 10 min; 2.) tetrahydrofurane, -78 deg C, 2.5 h; room temp., 1 h

2: 3-chloroperbenzoic acid / CHCl₃ / 0 deg C, overnight

3: sodium hydride / 0.75 h / Ambient temperature

With n-butyllithium; 3-chloro-benzenecarboperoxoic acid; sodium hydride; In chloroform;