Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-(2,2,2-trifluoroethyl phosphorochloridate)

Base Information

Chemical Name:Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-(2,2,2-trifluoroethyl phosphorochloridate)
CAS No.:114071-83-9
Molecular Formula:C₂₅H₃₂ClF₃N₅O₆PSi
Molecular Weight:650.066
Hs Code.:
Mol file:114071-83-9.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-(2,2,2-trifluoroethyl phosphorochloridate)

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Technology Process of Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-(2,2,2-trifluoroethyl phosphorochloridate)

There total 2 articles about Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-(2,2,2-trifluoroethyl phosphorochloridate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114071-79-3
C₂₈H₄₁F₃N₅O₆PSi₂

: 114071-83-9
Phosphorochloridic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-3-yl ester 2,2,2-trifluoro-ethyl ester

Guidance literature:: With sulfuryl dichloride; In dichloromethane; 1.) 0 deg C, 2.) 30 min, room temperature;
DOI:10.1016/S0040-4039(00)95534-5

Reference yield:

: 51549-39-4
N⁶-benzoyl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

: 114071-83-9
Phosphorochloridic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-3-yl ester 2,2,2-trifluoro-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: sulfuryl chloride / CH₂Cl₂ / 1.) 0 deg C, 2.) 30 min, room temperature

With sulfuryl dichloride; In dichloromethane;
DOI:10.1016/S0040-4039(00)95534-5