1,4-Butanediol, 2,2-dimethyl-, dimethanesulfonate

Base Information

Chemical Name:1,4-Butanediol, 2,2-dimethyl-, dimethanesulfonate
CAS No.:4239-25-2
Molecular Formula:C8H18O6S2
Molecular Weight:274.3549
Hs Code.:
NSC Number:53925
DSSTox Substance ID:DTXSID00962452
Wikidata:Q82944134

Synonyms:4239-25-2;1,4-Butanediol, 2,2-dimethyl-, dimethanesulfonate;NSC53925;DTXSID00962452;NSC 53925;NSC-53925;2,2-Dimethylbutane-1,4-diyl dimethanesulfonate;EN300-19464091;4-(methanesulfonyloxy)-2,2-dimethylbutyl methanesulfonate

Suppliers and Price of 1,4-Butanediol, 2,2-dimethyl-, dimethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,4-Butanediol, 2,2-dimethyl-, dimethanesulfonate

Chemical Property:

Vapor Pressure:3.36E-08mmHg at 25°C
Refractive Index:1.47
Boiling Point:459.8°Cat760mmHg
Flash Point:231.9°C
Density:1.273g/cm³
XLogP3:0.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:7
Exact Mass:274.05448064
Heavy Atom Count:16
Complexity:395

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(CCOS(=O)(=O)C)COS(=O)(=O)C

Technology Process of 1,4-Butanediol, 2,2-dimethyl-, dimethanesulfonate

There total 4 articles about 1,4-Butanediol, 2,2-dimethyl-, dimethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 32812-23-0
2,2-dimethylbutane-1,4-diol

: 124-63-0
methanesulfonyl chloride

: 4239-25-2
2,2-dimethyl-1,4-butanediyl dimesylate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 22 ℃; for 2h;
DOI:10.1021/acs.orglett.9b03887

Reference yield:

: 75-75-2,98527-29-8
methanesulfonic acid

: 32812-23-0
2,2-dimethylbutane-1,4-diol

: 4239-25-2
2,2-dimethyl-1,4-butanediyl dimesylate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

: 597-43-3
2,2-dimethylsuccinic acid

: 4239-25-2
2,2-dimethyl-1,4-butanediyl dimesylate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 - 20 °C

2: triethylamine / dichloromethane / 3 h / 0 - 20 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;