DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, methyl ester, mono(4-methylbenzenesulfonate)

Base Information

Chemical Name:DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, methyl ester, mono(4-methylbenzenesulfonate)
CAS No.:114531-64-5
Molecular Formula:C₇H₈O₃S*C₂₃H₂₄N₄O₅S
Molecular Weight:640.738
Hs Code.:
Mol file:114531-64-5.mol

Synonyms:

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Chemical Property of DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, methyl ester, mono(4-methylbenzenesulfonate)

Chemical Property:

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Technology Process of DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, methyl ester, mono(4-methylbenzenesulfonate)

There total 6 articles about DL-Phenylalanine, 3-(aminoiminomethyl)-N-[N-(2-naphthalenylsulfonyl)glycyl]-, methyl ester, mono(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 67-56-1
methanol

: 104-15-4
toluene-4-sulfonic acid

: 114531-56-5
Nα-(2-Naphthylsulfonylglycyl)-3-amidinophenylalanin

: 114531-64-5
3-(3-Carbamimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionic acid methyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: for 2.5h; Heating;

Reference yield:

: 63999-80-4
(+/-)-3-cyanophenylalanine

: 114531-64-5
3-(3-Carbamimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionic acid methyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 57 percent / 1M NaOH / ethyl acetate / 4 h / Ambient temperature

2: 95 percent / H₂S / pyridine; triethylamine / 48 h / Ambient temperature

3: 87 percent / acetone / 0.25 h / Heating

4: 77 percent / CH₃COONH₄ / methanol / 2.5 h / 60 °C

5: 75 percent / 2.5 h / Heating

With sodium hydroxide; hydrogen sulfide; ammonium acetate; In pyridine; methanol; ethyl acetate; triethylamine; acetone;

Reference yield:

: 92740-50-6
2-Naphthylsulfonylglycylchlorid

: 114531-64-5
3-(3-Carbamimidoyl-phenyl)-2-[2-(naphthalene-2-sulfonylamino)-acetylamino]-propionic acid methyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 57 percent / 1M NaOH / ethyl acetate / 4 h / Ambient temperature

2: 95 percent / H₂S / pyridine; triethylamine / 48 h / Ambient temperature

3: 87 percent / acetone / 0.25 h / Heating

4: 77 percent / CH₃COONH₄ / methanol / 2.5 h / 60 °C

5: 75 percent / 2.5 h / Heating

With sodium hydroxide; hydrogen sulfide; ammonium acetate; In pyridine; methanol; ethyl acetate; triethylamine; acetone;