4-Azido-N-{6-oxo-6-[(pyren-1-yl)amino]hexyl}benzamide

Base Information

Chemical Name:4-Azido-N-{6-oxo-6-[(pyren-1-yl)amino]hexyl}benzamide
CAS No.:115205-70-4
Molecular Formula:C₂₉H₂₅N₅O₂
Molecular Weight:475.55
Hs Code.:
DSSTox Substance ID:DTXSID50556446
Wikidata:Q82438000

Synonyms:115205-70-4;4-Azido-N-{6-oxo-6-[(pyren-1-yl)amino]hexyl}benzamide;DTXSID50556446

Suppliers and Price of 4-Azido-N-{6-oxo-6-[(pyren-1-yl)amino]hexyl}benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-Azido-N-{6-oxo-6-[(pyren-1-yl)amino]hexyl}benzamide

Chemical Property:

XLogP3:7.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:475.20082506
Heavy Atom Count:36
Complexity:819

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C3C(=C1)C=CC4=C(C=CC(=C43)C=C2)NC(=O)CCCCCNC(=O)C5=CC=C(C=C5)N=[N+]=[N-]

Technology Process of 4-Azido-N-{6-oxo-6-[(pyren-1-yl)amino]hexyl}benzamide

There total 4 articles about 4-Azido-N-{6-oxo-6-[(pyren-1-yl)amino]hexyl}benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6427-66-3
4-azidobenzoic acid

: 115205-70-4
N-<5-<(1-pyrenylamino)carbonyl>pentyl>-4-azidobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride

2: 74 percent / aq. NaOH / 20 h / 0 °C

3: triethylamine / CH₂Cl₂ / 4 h / 0 °C

4: triethylamine / CH₂Cl₂ / 0 °C

With sodium hydroxide; thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jo00250a017

Reference yield:

: 14848-01-2
4-azidobenzoyl chloride

: 115205-70-4
N-<5-<(1-pyrenylamino)carbonyl>pentyl>-4-azidobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / aq. NaOH / 20 h / 0 °C

2: triethylamine / CH₂Cl₂ / 4 h / 0 °C

3: triethylamine / CH₂Cl₂ / 0 °C

With sodium hydroxide; triethylamine; In dichloromethane;
DOI:10.1021/jo00250a017

Reference yield:

: 85287-36-1
6-<(4-Azidobenzoyl)amino>hexanoic acid

: 115205-70-4
N-<5-<(1-pyrenylamino)carbonyl>pentyl>-4-azidobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 4 h / 0 °C

2: triethylamine / CH₂Cl₂ / 0 °C

With triethylamine; In dichloromethane;
DOI:10.1021/jo00250a017