{[2-(Phenoxysulfonyl)phenyl]methylene}di(4,1-phenylene) diacetate

Base Information

Chemical Name:{[2-(Phenoxysulfonyl)phenyl]methylene}di(4,1-phenylene) diacetate
CAS No.:115511-92-7
Molecular Formula:C29H24O7S
Molecular Weight:516.571
Hs Code.:
DSSTox Substance ID:DTXSID00556734
Wikidata:Q82438404
Mol file:115511-92-7.mol

Synonyms:115511-92-7;DTXSID00556734;{[2-(Phenoxysulfonyl)phenyl]methylene}di(4,1-phenylene) diacetate

Suppliers and Price of {[2-(Phenoxysulfonyl)phenyl]methylene}di(4,1-phenylene) diacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of {[2-(Phenoxysulfonyl)phenyl]methylene}di(4,1-phenylene) diacetate

Chemical Property:

XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:10
Exact Mass:516.12427427
Heavy Atom Count:37
Complexity:808

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1=CC=C(C=C1)C(C2=CC=C(C=C2)OC(=O)C)C3=CC=CC=C3S(=O)(=O)OC4=CC=CC=C4

Technology Process of {[2-(Phenoxysulfonyl)phenyl]methylene}di(4,1-phenylene) diacetate

There total 4 articles about {[2-(Phenoxysulfonyl)phenyl]methylene}di(4,1-phenylene) diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 147510-56-3
Acetic acid 4-[(4-acetoxy-phenyl)-(2-chlorosulfonyl-phenyl)-methyl]-phenyl ester

: 108-95-2,27073-41-2
phenol

: 115511-92-7
bis(4.acetoxyphenyl)<2-(phenoxysulfonyl)phenyl>methane

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 12h;
DOI:10.1021/jm00118a020

Reference yield:

: 172464-36-7
2-(4,4'-dihydroxy-benzhydryl)-benzenesulfonic acid

: 115511-92-7
bis(4.acetoxyphenyl)<2-(phenoxysulfonyl)phenyl>methane

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / 1.) RT, 4h, 2.) CH₂Cl₂, 1 h

2: PCl₅ / 3 h / 60 - 65 °C / 0.1 Torr

3: 92 percent / Et₃N / CH₂Cl₂ / 12 h / 25 °C

With phosphorus pentachloride; triethylamine; In dichloromethane;
DOI:10.1021/jm00118a020

Reference yield:

: 34487-61-1
phenolsulphophthaleine sodium salt

: 115511-92-7
bis(4.acetoxyphenyl)<2-(phenoxysulfonyl)phenyl>methane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaBH₄, 2.) 5percent HCl / aq. ethanol / 48 h / 25 °C

2: 72 percent / 1.) RT, 4h, 2.) CH₂Cl₂, 1 h

3: PCl₅ / 3 h / 60 - 65 °C / 0.1 Torr

4: 92 percent / Et₃N / CH₂Cl₂ / 12 h / 25 °C

With hydrogenchloride; sodium tetrahydroborate; phosphorus pentachloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm00118a020