Germanium, (tetrahydro-2-methylfuran)bis(2,4,6-trimethylphenyl)-

Base Information

• Chemical Name: Germanium, (tetrahydro-2-methylfuran)bis(2,4,6-trimethylphenyl)-
• CAS No.: 115590-26-6
• Molecular Formula: C₅H₁₀O*C₁₈H₂₂Ge
• Molecular Weight: 397.096
• Mol file: 115590-26-6.mol

Synonyms:

Chemical Property of Germanium, (tetrahydro-2-methylfuran)bis(2,4,6-trimethylphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Germanium, (tetrahydro-2-methylfuran)bis(2,4,6-trimethylphenyl)-

There total 2 articles about Germanium, (tetrahydro-2-methylfuran)bis(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyltetrahydrofuran (96-47-9) + dimesitylbis(trimethylsilyl)germane (111655-80-2) → dimesitylgermylene (2-methyl)tetrahydrofuran complex (115590-26-6)

Guidance literature:

In solid matrix; Irradiation (UV/VIS); quartz UV cell, degassing by three freeze-pump-thaw cycles, irradn. with a low pressure mercury lamp (254 nm) at 77K in 3-MP/IP (3-methylpentane/isopentane) solid matrix; not isolated, detd. by UV;

Reference yield:

2-methyltetrahydrofuran (96-47-9) + bis(2,4,6-trimethylphenyl)germylene (72176-49-9) → dimesitylgermylene(1-methyltetrahydrofuran) (115590-26-6)

Guidance literature:

In further solvent(s); equil.; Ge species not isolated;

upstream raw materials:

2-methyltetrahydrofuran

bis(2,4,6-trimethylphenyl)germylene

dimesitylbis(trimethylsilyl)germane

Refernces