5-Iodo-2-methoxybenzoyl chloride

Base Information

Chemical Name:5-Iodo-2-methoxybenzoyl chloride
CAS No.:115860-69-0
Molecular Formula:C8H6ClIO2
Molecular Weight:296.492
Hs Code.:
DSSTox Substance ID:DTXSID50557271
Wikidata:Q82439128

Synonyms:115860-69-0;5-iodo-2-methoxybenzoyl chloride;SCHEMBL4733642;DTXSID50557271

Suppliers and Price of 5-Iodo-2-methoxybenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5-Iodo-2-methoxybenzoyl chloride

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:295.91010
Heavy Atom Count:12
Complexity:174

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)I)C(=O)Cl

Technology Process of 5-Iodo-2-methoxybenzoyl chloride

There total 2 articles about 5-Iodo-2-methoxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2786-00-7
2-methoxy-5-iodobenzoic acid

: 115860-69-0
2-methoxy-5-iodobenzoyl chloride

Guidance literature:: With thionyl chloride;
DOI:10.1021/jm00174a003

Reference yield:

: 40757-09-3
methyl 2-methoxy-5-iodobenzoate

: 115860-69-0
2-methoxy-5-iodobenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / methanol; H₂O / 2 h / Heating

2: SOCl₂ / 16 h / Heating

With potassium hydroxide; thionyl chloride; In methanol; water;
DOI:10.1021/ol0615228