Carbamic acid, [4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2,5-dioxo-1-pyrrolidinyl)oxy ]carbonyl]butyl]-, phenylmethyl ester, (S)-

Base Information

Chemical Name:Carbamic acid, [4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2,5-dioxo-1-pyrrolidinyl)oxy ]carbonyl]butyl]-, phenylmethyl ester, (S)-
CAS No.:116115-11-8
Molecular Formula:C22H29N3O8
Molecular Weight:463.488
Hs Code.:
Mol file:116115-11-8.mol

Synonyms:

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Chemical Property of Carbamic acid, [4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2,5-dioxo-1-pyrrolidinyl)oxy ]carbonyl]butyl]-, phenylmethyl ester, (S)-

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Technology Process of Carbamic acid, [4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2,5-dioxo-1-pyrrolidinyl)oxy ]carbonyl]butyl]-, phenylmethyl ester, (S)-

There total 1 articles about Carbamic acid, [4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2,5-dioxo-1-pyrrolidinyl)oxy ]carbonyl]butyl]-, phenylmethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 7733-29-1,199924-46-4
Z-Orn(Boc)-OH

: 116115-11-8
(S)-2-Benzyloxycarbonylamino-5-tert-butoxycarbonylamino-pentanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 10h;
DOI:10.1021/jo990769y

Reference yield: 51.0%

: 2482-00-0
agmatine sulphate

: 116115-11-8
(S)-2-Benzyloxycarbonylamino-5-tert-butoxycarbonylamino-pentanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

: Z-Orn(Boc)-Agm*0.5H₂SO₄

Guidance literature:: With triethylamine; In water; acetonitrile;
DOI:10.1016/S0968-0896(97)00105-3

Reference yield:

: 116115-11-8
(S)-2-Benzyloxycarbonylamino-5-tert-butoxycarbonylamino-pentanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 2-(2-benzyloxycarbonylamino-5-tert-butoxycarbonylamino-pentanoylamino)-5-tert-butoxycarbonylamino-pentanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / H₂O; tetrahydrofuran / 6 h / 20 °C

2: dicyclohexylcarbodiimide / tetrahydrofuran

With sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; water; 1: Substitution / 2: Esterification;
DOI:10.1021/jo990769y