9-Dodecylphenanthrene

Base Information

• Chemical Name: 9-Dodecylphenanthrene
• CAS No.: 3788-61-2
• Molecular Formula: C₂₆H₃₄
• Molecular Weight: 346.556
• NSC Number: 107103
• DSSTox Substance ID: DTXSID80296020
• Nikkaji Number: J104.846E
• Wikidata: Q82036319
• Mol file: 3788-61-2.mol

Synonyms:9-Dodecylphenanthrene;Phenanthrene, 9-dodecyl-;9-n-Dodecylphenanthrene;3788-61-2;NSC 107103;NSC107103;9-Dodecylphenanthrene #;9-n-Dodecyl-phenanthrene;DTXSID80296020;STK365513;AKOS005442947;NSC-107103

Chemical Property of 9-Dodecylphenanthrene

Chemical Property:

• Vapor Pressure: 2.74E-09mmHg at 25°C
• Refractive Index: 1.5220 (estimate)
• Boiling Point: 490.5°Cat760mmHg
• Flash Point: 250.6°C
• PSA: 0.00000
• Density: 0.974g/cm³
• LogP: 8.45640
• XLogP3: 10.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 11
• Exact Mass: 346.266051085
• Heavy Atom Count: 26
• Complexity: 359

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCC1=CC2=CC=CC=C2C3=CC=CC=C31

Technology Process of 9-Dodecylphenanthrene

There total 3 articles about 9-Dodecylphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-[9]phenanthryl-dodecan-1-one (412025-93-5) → 9-Docecyl-phenanthren (3788-61-2)

Guidance literature:

With ethanol; sodium methylate; hydrazine hydrate; at 200 ℃;

DOI:10.1021/ja01182a029

Reference yield:

lauric acid (143-07-7) → 9-Docecyl-phenanthren (3788-61-2)

Guidance literature:

Multi-step reaction with 3 steps

1: phosphoric acid; NH₃ / 290 - 300 °C

2: diethyl ether; benzene / anschliessend Behandeln mit Eis und Schwefelsaeure

3: hydrazine hydrate; sodium methylate; ethanol / 200 °C

With diethyl ether; ethanol; phosphoric acid; ammonia; sodium methylate; hydrazine hydrate; benzene;

DOI:10.1021/ja01182a029

Reference yield:

undecyl cyanide (2437-25-4) → 9-Docecyl-phenanthren (3788-61-2)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; benzene / anschliessend Behandeln mit Eis und Schwefelsaeure

2: hydrazine hydrate; sodium methylate; ethanol / 200 °C

With diethyl ether; ethanol; sodium methylate; hydrazine hydrate; benzene;

DOI:10.1021/ja01182a029

upstream raw materials:

1-[9]phenanthryl-dodecan-1-one

lauric acid

undecyl cyanide

Downstream raw materials:

9-Dodecyltetradecahydrophenanthrene