5H-1,3,4-Oxadiazolo[3,2-a][1,3,5]triazine-5,7(6H)-dithione, 2-(4-chlorophenyl)-6-[(5-fluoro-2-methylphenyl)sulfonyl]-

Base Information

Chemical Name:5H-1,3,4-Oxadiazolo[3,2-a][1,3,5]triazine-5,7(6H)-dithione, 2-(4-chlorophenyl)-6-[(5-fluoro-2-methylphenyl)sulfonyl]-
CAS No.:116221-96-6
Molecular Formula:C₁₇H₁₀ClFN₄O₃S₃
Molecular Weight:468.941
Hs Code.:
Mol file:116221-96-6.mol

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Chemical Property of 5H-1,3,4-Oxadiazolo[3,2-a][1,3,5]triazine-5,7(6H)-dithione, 2-(4-chlorophenyl)-6-[(5-fluoro-2-methylphenyl)sulfonyl]-

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Technology Process of 5H-1,3,4-Oxadiazolo[3,2-a][1,3,5]triazine-5,7(6H)-dithione, 2-(4-chlorophenyl)-6-[(5-fluoro-2-methylphenyl)sulfonyl]-

There total 2 articles about 5H-1,3,4-Oxadiazolo[3,2-a][1,3,5]triazine-5,7(6H)-dithione, 2-(4-chlorophenyl)-6-[(5-fluoro-2-methylphenyl)sulfonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 445-05-6
5-fluoro-2-methylbenzenesulfonyl chloride

: 116221-91-1
2-p-chlorophenyl-1,3,4-oxadiazolo<3,2-a>-s-triazine-5,7-(6H)-dithione

: 116221-96-6
2-p-chlorophenyl-6-(2-methyl-5-fluorophenyl)-1,3,4-oxadiazolo<3,2-a>-s-triazine-5,7-dithione

Guidance literature:: With pyridine; at 100 ℃; for 1.5h;

Reference yield:

: 89335-12-6
N¹-(5-p-chlorophenyl-1,3,4-oxadiazol-2-yl)thiourea

: 116221-96-6
2-p-chlorophenyl-6-(2-methyl-5-fluorophenyl)-1,3,4-oxadiazolo<3,2-a>-s-triazine-5,7-dithione

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / ethanol / 6 h / Heating

2: 69 percent / pyridine / 1.5 h / 100 °C

With pyridine; In ethanol;