4-methylphenyl dimethoxyphosphanecarboxylate oxide

Base Information

• Chemical Name: 4-methylphenyl dimethoxyphosphanecarboxylate oxide
• CAS No.: 72305-97-6
• Molecular Formula: C10H13O5P
• Molecular Weight: 244.184

Synonyms:

Chemical Property of 4-methylphenyl dimethoxyphosphanecarboxylate oxide

Chemical Property:

• Vapor Pressure: 0.000779mmHg at 25°C
• Boiling Point: 306.3°Cat760mmHg
• Flash Point: 152.9°C
• Density: 1.241g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methylphenyl dimethoxyphosphanecarboxylate oxide

There total 2 articles about 4-methylphenyl dimethoxyphosphanecarboxylate oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

p-tolyl chloroformate (937-62-2) → dimethyl p-tolyloxycarbonylphosphonate (72305-97-6)

Guidance literature:

With phosphorous acid trimethyl ester;

Reference yield: 93.0%

p-tolyl chloroformate (937-62-2) + phosphorous acid trimethyl ester (121-45-9) → dimethyl p-tolyloxycarbonylphosphonate (72305-97-6)

Guidance literature:

DOI:10.1021/jm00356a028

Reference yield: 87.0%

dimethyl p-tolyloxycarbonylphosphonate (72305-97-6) → C8H7O5P(2-)*2Na(1+) (74270-31-8)

Guidance literature:

With trimethylsilyl bromide; Amberlite IRC 50 (Na⁺ form); for 3h; Ambient temperature;

DOI:10.1021/jm00356a028

upstream raw materials:

p-tolyl chloroformate

phosphorous acid trimethyl ester

Downstream raw materials:

C₈H₇O₅P^(2-)*2Na⁽¹⁺⁾

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