Benzenesulfinic acid, cyclohexyl ester

Base Information

• Chemical Name: Benzenesulfinic acid, cyclohexyl ester
• CAS No.: 116544-95-7
• Molecular Formula: C12H16O2S
• Molecular Weight: 224.324
• Mol file: 116544-95-7.mol

Synonyms:

Chemical Property of Benzenesulfinic acid, cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenesulfinic acid, cyclohexyl ester

There total 2 articles about Benzenesulfinic acid, cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

thiophenol (108-98-5) + cyclohexanol (108-93-0) → cyclohexyl benzenesulfinate (116544-95-7)

Guidance literature:

With tetrabutylammonium tetrafluoroborate; In dichloromethane; at 20 ℃; for 20h; Electrochemical reaction; Inert atmosphere; Green chemistry;

DOI:10.1039/c9gc02125f

Reference yield:

diphenyldisulfane (882-33-7) + cyclohexanol (108-93-0) → cyclohexyl benzenesulfinate (116544-95-7)

Guidance literature:

With N-Bromosuccinimide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) 0 deg C, 20 min., 2.) 20 deg C, 60 min.,;

DOI:10.1055/s-1988-27535

upstream raw materials:

diphenyldisulfane

cyclohexanol

thiophenol