Piperidine, 1-[3-(2,4-dichlorophenyl)-1-oxo-2-propenyl]-, (E)-

Base Information

Chemical Name:Piperidine, 1-[3-(2,4-dichlorophenyl)-1-oxo-2-propenyl]-, (E)-
CAS No.:116591-86-7
Molecular Formula:C14H15Cl2NO
Molecular Weight:284.18100
Hs Code.:
Mol file:116591-86-7.mol

Synonyms:(E)-3-(2,4-Dichloro-phenyl)-1-piperidin-1-yl-propenone;

Suppliers and Price of Piperidine, 1-[3-(2,4-dichlorophenyl)-1-oxo-2-propenyl]-, (E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Piperidine, 1-[3-(2,4-dichlorophenyl)-1-oxo-2-propenyl]-, (E)-

Chemical Property:

PSA：20.31000
LogP:3.95700

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Piperidine, 1-[3-(2,4-dichlorophenyl)-1-oxo-2-propenyl]-, (E)-

There total 3 articles about Piperidine, 1-[3-(2,4-dichlorophenyl)-1-oxo-2-propenyl]-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 874-42-0
2,4-dichlorobenzaldeyhde

: 146060-34-6
fluoroiodomethyl piperidino ketone

: 116591-86-7
(E)-2-(2,4-dichlorophenyl)vinyl piperidino ketone

: 146060-53-9,146060-54-0
2-(2,4-dichlorophenyl)-1-fluorovinyl piperidino ketone

Guidance literature:: With triethylarsine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 110 ℃; for 24h;

Reference yield: 14.0%

: 874-42-0
2,4-dichlorobenzaldeyhde

: 146060-34-6
fluoroiodomethyl piperidino ketone

: 116591-86-7
(E)-2-(2,4-dichlorophenyl)vinyl piperidino ketone

: 146060-54-0
(E)-2-(2,4-dichlorophenyl)-1-fluorovinyl piperidino ketone

: 146060-53-9
(Z)-2-(2,4-dichlorophenyl)-1-fluorovinyl piperidino ketone

Guidance literature:: With triethylarsine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 110 ℃; for 24h; Yield given. Title compound not separated from byproducts;

Reference yield:

: 321-77-7
fluorochloromethyl piperidino ketone

: 116591-86-7
(E)-2-(2,4-dichlorophenyl)vinyl piperidino ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaI / acetone / 72 h / Heating

2: 14 percent / triethylarsine / Pd(PPh₃)4 / 24 h / 110 °C

With triethylarsine; sodium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In acetone;