N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine

Base Information

Chemical Name:N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine
CAS No.:118498-98-9
Molecular Formula:C20H22N2
Molecular Weight:290.408
Hs Code.:2933990090
DSSTox Substance ID:DTXSID40383182
ChEMBL ID:CHEMBL522239
Mol file:118498-98-9.mol

Synonyms:118498-98-9;N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine;AURORA KA-7529;Oprea1_213867;Oprea1_420674;CBDivE_004284;CHEMBL522239;SCHEMBL5456604;DTXSID40383182;QFDFWFMCDCUQNX-UHFFFAOYSA-N;Benzyl-(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-amine;STK530129;AKOS001623179;AKOS022184478;1benzylamino 6methyl 2,3,4,9tetrahydro1h carbazole

Suppliers and Price of N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-BENZYL-6-METHYL-2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-AMINE 95.00%
5MG
$ 504.67

Total 5 raw suppliers

Chemical Property of N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine

Chemical Property:

Vapor Pressure:1.26E-09mmHg at 25°C
Boiling Point:486.8oC at 760 mmHg
Flash Point:248.2oC
PSA：27.82000
Density:1.16g/cm3
LogP:5.03440
XLogP3:4.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:290.178298710
Heavy Atom Count:22
Complexity:363

Purity/Quality:

99.90% ^*data from raw suppliers

N-BENZYL-6-METHYL-2,3,4,9-TETRAHYDRO-1H-CARBAZOL-1-AMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)NC3=C2CCCC3NCC4=CC=CC=C4

Technology Process of N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine

There total 8 articles about N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 3449-48-7,812649-03-9
6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one

: 100-46-9
benzylamine

: 118498-98-9
N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine

Guidance literature:: 6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one; benzylamine; With toluene-4-sulfonic acid; In toluene; at 140 ℃; for 16h; Dean-Stark; Inert atmosphere;

With sodium tetrahydroborate; In methanol; at 0 - 80 ℃;
DOI:10.1016/j.ejmech.2018.11.016

Reference yield:

: 115174-30-6
1-benzylimino-6-methyl-1,2,3,4-tetrahydrocarbazole

: 118498-98-9
N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 4h;
DOI:10.1007/BF00472254

Reference yield:

: 3449-48-7,812649-03-9
6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one

: 118498-98-9
N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / xylene / 3 h / Heating

2: NaBH₄ / ethanol / 1 h / 20 °C

With sodium tetrahydroborate; In ethanol; xylene;
DOI:10.1007/BF00763273