N-benzyl-N-(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-yl)acetamide

Base Information

Chemical Name:N-benzyl-N-(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-yl)acetamide
CAS No.:115174-37-3
Molecular Formula:C22H24N2O
Molecular Weight:332.43900
Hs Code.:
Mol file:115174-37-3.mol

Synonyms:N-benzyl-N-(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-yl)acetamide;N-Benzyl-N-(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-acetamide;

Suppliers and Price of N-benzyl-N-(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-yl)acetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-yl)acetamide

Chemical Property:

PSA：36.10000
LogP:4.90240

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-benzyl-N-(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-yl)acetamide

There total 5 articles about N-benzyl-N-(6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 118498-98-9
N-benzyl-6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-amine

: 75-36-5
acetyl chloride

: 115174-37-3
N-benzyl-N-(6-methyl-1,2,3,4-tetrahydro-1-carbazolyl)acetamide

Guidance literature:: With triethylamine; In toluene; at 20 ℃; for 1h;
DOI:10.1007/BF00472254

Reference yield:

: 3449-48-7,812649-03-9
6-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one

: 115174-37-3
N-benzyl-N-(6-methyl-1,2,3,4-tetrahydro-1-carbazolyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / xylene / 3 h / Heating

2: NaBH₄ / ethanol / 4 h / 20 °C

3: 87 percent / triethylamine / toluene / 1 h / 20 °C

With sodium tetrahydroborate; triethylamine; In ethanol; toluene; xylene;
DOI:10.1007/BF00472254

Reference yield:

: 115174-30-6
1-benzylimino-6-methyl-1,2,3,4-tetrahydrocarbazole

: 115174-37-3
N-benzyl-N-(6-methyl-1,2,3,4-tetrahydro-1-carbazolyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / ethanol / 4 h / 20 °C

2: 87 percent / triethylamine / toluene / 1 h / 20 °C

With sodium tetrahydroborate; triethylamine; In ethanol; toluene;
DOI:10.1007/BF00472254