1H-Inden-1-ol, 2,3-dihydro-, 4-nitrobenzoate

Base Information

• Chemical Name: 1H-Inden-1-ol, 2,3-dihydro-, 4-nitrobenzoate
• CAS No.: 119959-31-8
• Molecular Formula: C16H13NO4
• Molecular Weight: 283.284
• Mol file: 119959-31-8.mol

Synonyms:

Chemical Property of 1H-Inden-1-ol, 2,3-dihydro-, 4-nitrobenzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Inden-1-ol, 2,3-dihydro-, 4-nitrobenzoate

There total 6 articles about 1H-Inden-1-ol, 2,3-dihydro-, 4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-chloroindane (35275-62-8) → (+/-)-1-(p-nitrobenzoyloxy)indane (119959-31-8)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium acetate; aqueous acetic acid

2: ethanolic KOH

With potassium hydroxide; potassium acetate; acetic acid;

DOI:10.1021/ja01256a050

Reference yield:

trans-2-bromo-1-indanol (10368-44-2,78684-69-2) → (+/-)-1-(p-nitrobenzoyloxy)indane (119959-31-8)

Guidance literature:

Multi-step reaction with 2 steps

1: platinized Raney nickel; MgCl₂; aq.-ethanolic KOH / Hydrogenolyse

With potassium hydroxide; platinized Raney nickel; magnesium chloride;

DOI:10.1021/ja01256a050

Reference yield:

inden-1-one (83-33-0) → (+/-)-1-(p-nitrobenzoyloxy)indane (119959-31-8)

Guidance literature:

Multi-step reaction with 2 steps

1: platinized Raney nickel; ethanolic NaOH / Hydrogenation

With sodium hydroxide; platinized Raney nickel;

DOI:10.1021/ja01256a050

upstream raw materials:

1-Indanol

1-chloroindane

trans-2-bromo-1-indanol

inden-1-one

Downstream raw materials:

1-indene

Refernces

• 1、 Chen, Kun-Quan,Shen, Jie,Wang, Zhi-Xiang,Chen, Xiang-Yu. "A donor-acceptor complex enables the synthesis of: E -olefins from alcohols, amines and carboxylic acids". . p. 6684 - 6690. Retrieved 2021/05/31.