Ethyl 4-diethoxyphosphoryl-2-methylbut-2-enoate

Base Information

Chemical Name:Ethyl 4-diethoxyphosphoryl-2-methylbut-2-enoate
CAS No.:122009-11-4
Molecular Formula:C11H21O5P
Molecular Weight:264.259
Hs Code.:
European Community (EC) Number:601-818-6
DSSTox Substance ID:DTXSID301234859
Mol file:122009-11-4.mol

Synonyms:122009-11-4;SCHEMBL5873561;DTXSID301234859;Ethyl 4-(diethoxyphosphinyl)-2-methyl-2-butenoate

Suppliers and Price of Ethyl 4-diethoxyphosphoryl-2-methylbut-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Ethyl 4-diethoxyphosphoryl-2-methylbut-2-enoate

Chemical Property:

Vapor Pressure:6.2E-05mmHg at 25°C
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:9
Exact Mass:264.11266076
Heavy Atom Count:17
Complexity:301

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=CCP(=O)(OCC)OCC)C

Technology Process of Ethyl 4-diethoxyphosphoryl-2-methylbut-2-enoate

There total 3 articles about Ethyl 4-diethoxyphosphoryl-2-methylbut-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107-20-0
2-chloroethanal

: 105-37-3,20741-13-3
Ethyl propionate

: 122-52-1
triethyl phosphite

: 122009-11-4
ethyl 4-diethoxyphosphono-2-methyl-2-butenoate

Guidance literature:: With ammonium bromide; In water; acetonitrile; at 100 ℃; for 12h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere;

Reference yield: 95.0%

: 50471-46-0
ethyl 2-methyl-2-hydroxy-3-butenoate

: 122-52-1
triethyl phosphite

: 122009-11-4
ethyl 4-diethoxyphosphono-2-methyl-2-butenoate

Guidance literature:: With methyl(tributyl)phosphonium iodide; at 120 ℃; Inert atmosphere;

Reference yield: 87.41%

: 27772-62-9
ethyl 2-formylpropionate

: 1660-94-2
Tetraethyl methylenediphosphonate

: 122009-11-4
ethyl 4-diethoxyphosphono-2-methyl-2-butenoate

Guidance literature:: Tetraethyl methylenediphosphonate; With sodium methylate; In tetrahydrofuran; at 10 - 30 ℃; for 1.5h; Inert atmosphere;

ethyl 2-formylpropionate; In tetrahydrofuran; at 35 ℃; for 2h; Solvent; Temperature; Reagent/catalyst;