Morpholine, 4,4'-(3-pyridinylmethylene)bis-

Base Information

Chemical Name:Morpholine, 4,4'-(3-pyridinylmethylene)bis-
CAS No.:122713-47-7
Molecular Formula:C14H21N3O2
Molecular Weight:263.34
Hs Code.:
DSSTox Substance ID:DTXSID20354315
Wikidata:Q82132378
Mol file:122713-47-7.mol

Synonyms:122713-47-7;Morpholine, 4,4'-(3-pyridinylmethylene)bis-;4,4'-(pyridin-3-ylmethylene)dimorpholine;CDS1_000586;Maybridge1_002874;Oprea1_449685;Oprea1_557393;CBDivE_002787;DivK1c_001626;F0138-4744;HMS549K14;DTXSID20354315;STK366720;AKOS000650991;CCG-243572;SDCCGMLS-0064698.P001;4,4'-(3-Pyridinylmethylene)dimorpholine;4,4'-(pyridin-3-ylmethanediyl)dimorpholine;4-[(MORPHOLIN-4-YL)(PYRIDIN-3-YL)METHYL]MORPHOLINE

Suppliers and Price of Morpholine, 4,4'-(3-pyridinylmethylene)bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Morpholine, 4,4'-(3-pyridinylmethylene)bis-

Chemical Property:

XLogP3:0.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:263.16337692
Heavy Atom Count:19
Complexity:247

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCN1C(C2=CN=CC=C2)N3CCOCC3

Technology Process of Morpholine, 4,4'-(3-pyridinylmethylene)bis-

There total 1 articles about Morpholine, 4,4'-(3-pyridinylmethylene)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 500-22-1
3-pyridinecarboxaldehyde

: 13368-42-8
4-(trimethylsilyl)morpholine

: 107-46-0
Hexamethyldisiloxane

: 122713-47-7
3-(dimorpholinomethyl)pyridine

Guidance literature:: With bromine; trimethylsilyl trifluoromethanesulfonate; In tetrachloromethane; for 10h; Ambient temperature;

Reference yield:

: 122713-47-7
3-(dimorpholinomethyl)pyridine

: NE-10864

Guidance literature:: Multi-step reaction with 4 steps

1: 41 percent / TFA / tetrahydrofuran / Heating

2: 99 percent / TMSBr; H₂O

3: 52 percent / Na₂WO₄; H₂O₂

4: 61 percent / H₂; NaOH / Pd / H₂O

With sodium hydroxide; sodium tungstate; trimethylsilyl bromide; water; hydrogen; dihydrogen peroxide; trifluoroacetic acid; palladium; In tetrahydrofuran; water; 1: Condensation / 2: Hydrolysis / 3: Epoxidation / 4: Hydrogenation;