Benzenamine, 2-(3-pyridinylethynyl)-

Base Information

Chemical Name:Benzenamine, 2-(3-pyridinylethynyl)-
CAS No.:124643-40-9
Molecular Formula:C13H10N2
Molecular Weight:194.236
Hs Code.:
DSSTox Substance ID:DTXSID20464347
Nikkaji Number:J2.157.781B
Wikidata:Q82289635
Mol file:124643-40-9.mol

Synonyms:Benzenamine, 2-(3-pyridinylethynyl)-;124643-40-9;2-(3-pyridinylethynyl)aniline;SCHEMBL3840129;DTXSID20464347;[2-(2-pyridin-3-yl-ethynyl)-phenyl]-amine

Suppliers and Price of Benzenamine, 2-(3-pyridinylethynyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzenamine, 2-(3-pyridinylethynyl)-

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:194.084398327
Heavy Atom Count:15
Complexity:260

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C#CC2=CN=CC=C2)N

Technology Process of Benzenamine, 2-(3-pyridinylethynyl)-

There total 6 articles about Benzenamine, 2-(3-pyridinylethynyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1120-90-7
3-iodopyridine

: 103529-16-4
2-[(trimethylsilyl)ethynyl]aniline

: 124643-40-9
o-[2-(pyridin-3-yl)ethynyl]aniline

Guidance literature:: With tetrabutyl-ammonium chloride; sodium acetate; tris-(o-tolyl)phosphine; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 0.25h; microwave irradiation;
DOI:10.1016/j.tet.2005.01.032

Reference yield: 80.0%

: 626-55-1,163928-56-1
3-Bromopyridine

: 52670-38-9
2-ethynylaniline

: 124643-40-9
o-[2-(pyridin-3-yl)ethynyl]aniline

Guidance literature:: With copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; diisopropylamine; tri tert-butylphosphoniumtetrafluoroborate; In 1,4-dioxane; at 25 ℃; Inert atmosphere;
DOI:10.1021/jm101101q

Reference yield: 67.0%

: 52670-38-9
2-ethynylaniline

: 107658-27-5
pyridin-3-yl trifluoromethanesulfonate

: 124643-40-9
o-[2-(pyridin-3-yl)ethynyl]aniline

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 90 ℃; for 5h;
DOI:10.1016/S0040-4039(01)80456-1