Thionyl imide, N,N'-tellurobis-

Base Information

Chemical Name:Thionyl imide, N,N'-tellurobis-
CAS No.:124824-09-5
Molecular Formula:N2O2S2Te
Molecular Weight:251.744
Hs Code.:

Synonyms:

Suppliers and Price of Thionyl imide, N,N'-tellurobis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Thionyl imide, N,N'-tellurobis-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Thionyl imide, N,N'-tellurobis-

There total 1 articles about Thionyl imide, N,N'-tellurobis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: Hg(NSO)2

: 83665-28-5
bis(trifluoromethylthio)tellurium

: 124824-09-5
bis(sulfinylamido)tellurane

: 21259-75-6
mercury bis(trifluoromethanethiolate)

Guidance literature:: In carbon disulfide; Ar atmosphere, condensation of Te(SCF3)2 into a Carius tube containing asoln. of Hg(NSO)2, 50°C with exclusion of light (5 d), cooling t o -30°C; decantation, condensation of CS2, decantation at -30°C, drying (20°C (vacuum, 24 h), sublimation (55°C, 1E-3 Torr);

Reference yield: 1.0%

: 124824-09-5
bis(sulfinylamido)tellurane

: 7647-18-9
antimonypentachloride

: Cl(x)Te(x)

: NSNSTeCl*Cl*SbCl₃ = NSNSTeClClSbCl₃

: 10025-91-9
antimony(III) chloride

Guidance literature:: In dichloromethane; byproducts: SO2, N2; stirring mixt. of Te-compd. and SbCl5 (molar ratio 2.1:1.5) in abs. CH2Cl2 at -80°C in a sealed tube (12 h); filtration of pptn. in absence of air and moisture, washing (CH2Cl2), concn. of combined filtrates by removal of solvent in vac. to half of vol., crystn. after few weeks;